Design, synthesis, and characterization of 6-[(trimethyl)silylethynyl]naphthalene-2-ethene: a new precursor for the preparation of high-refractive-index organic materials

A new polymerizable naphthalene derivative has been designed, prepared, and characterized by H, C NMR, and MS. The new monomer synthesis has successfully been accomplished from a cheap commercially available raw material, in only four steps with good yields. The four steps can be easily scaled up fo...

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Bibliographic Details
Published inZeitschrift für Naturforschung. B, A journal of chemical sciences Vol. 75; no. 4; pp. 359 - 363
Main Authors Legrand, Sacha, Hannu-Kuure, Milja, Kärkkäinen, Ari
Format Journal Article
LanguageEnglish
Published BERLIN De Gruyter 28.04.2020
Walter De Gruyter
Subjects
Chemistry
Chemistry, Inorganic & Nuclear
Chemistry, Organic
high refractive index
monomer
Physical Sciences
Science & Technology
Sonogashira
synthesis
Wittig
synthesis
POLYMERS
Sonogashira
Wittig
high refractive index
monomer
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Summary:A new polymerizable naphthalene derivative has been designed, prepared, and characterized by H, C NMR, and MS. The new monomer synthesis has successfully been accomplished from a cheap commercially available raw material, in only four steps with good yields. The four steps can be easily scaled up for manufacturing purposes. It is anticipated that the new precursor can be very useful in the preparation of valuable materials with high refractive index for numerous opto-electronic applications.
ISSN:0932-0776
1865-7117
DOI:10.1515/znb-2019-0199