Synthesis of new transition metal complexes of 1H-perimidine derivatives having antimicrobial and anti-inflammatory activities
New series of 1 H -perimidine-2-thiol derivatives and (2-substituted-1 H -perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C 24 H 14 N 4 S 2 O 2 ) H 2 L 1 and (C 26 H 18 N 4 S 2 O 2 ) H 2 L 2 have been synthesized with transition metal ions, e.g., Copper (II), Silver (I), Cobalt (II) a...
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| Published in | Research on chemical intermediates Vol. 38; no. 7; pp. 1527 - 1550 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Dordrecht
Springer Netherlands
01.09.2012
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| Subjects | |
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| Abstract | New series of 1
H
-perimidine-2-thiol derivatives and (2-substituted-1
H
-perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C
24
H
14
N
4
S
2
O
2
) H
2
L
1
and (C
26
H
18
N
4
S
2
O
2
) H
2
L
2
have been synthesized with transition metal ions, e.g., Copper (II), Silver (I), Cobalt (II) and Ruthenium (III) were prepared and evaluated for their antimicrobial, analgesic and anti-inflammatory activities. The synthesized compounds and their complexes were characterized by elemental analysis,
1
H NMR, IR, MS, molar conductance, thermal gravimetric analysis and electronic spectra. All results revealed that compounds
3
and
13
exhibited high inhibitory effects against some bacterial strains by the disc diffusion method. On the other hand, compounds
2
,
3
,
7
and
12
displayed potent anti-inflammatory activity. |
|---|---|
| AbstractList | New series of 1
H
-perimidine-2-thiol derivatives and (2-substituted-1
H
-perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C
24
H
14
N
4
S
2
O
2
) H
2
L
1
and (C
26
H
18
N
4
S
2
O
2
) H
2
L
2
have been synthesized with transition metal ions, e.g., Copper (II), Silver (I), Cobalt (II) and Ruthenium (III) were prepared and evaluated for their antimicrobial, analgesic and anti-inflammatory activities. The synthesized compounds and their complexes were characterized by elemental analysis,
1
H NMR, IR, MS, molar conductance, thermal gravimetric analysis and electronic spectra. All results revealed that compounds
3
and
13
exhibited high inhibitory effects against some bacterial strains by the disc diffusion method. On the other hand, compounds
2
,
3
,
7
and
12
displayed potent anti-inflammatory activity. New series of 1H-perimidine-2-thiol derivatives and (2-substituted-1H-perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C24H14N4S2O2) H2L1 and (C26H18N4S2O2) H2L2 have been synthesized with transition metal ions, e.g., Copper (II), Silver (I), Cobalt (II) and Ruthenium (III) were prepared and evaluated for their antimicrobial, analgesic and anti-inflammatory activities. The synthesized compounds and their complexes were characterized by elemental analysis, H-1 NMR, IR, MS, molar conductance, thermal gravimetric analysis and electronic spectra. All results revealed that compounds 3 and 13 exhibited high inhibitory effects against some bacterial strains by the disc diffusion method. On the other hand, compounds 2, 3, 7 and 12 displayed potent anti-inflammatory activity. |
| Author | Rehim, Mohamed E. Abdel Abu-Bakr, Sherifa M. Hegab, Khaled H. El-Eraky, Wafaa El Beih, Ahmed A. Bassyouni, Fatma A. |
| Author_xml | – sequence: 1 givenname: Fatma A. surname: Bassyouni fullname: Bassyouni, Fatma A. email: fatma.nrc@hotmail.com organization: Chemistry Department of Natural and Microbial Products and Pharmaceutical Research Department, Center of Excellence for Advanced Sciences, National Research Centre – sequence: 2 givenname: Sherifa M. surname: Abu-Bakr fullname: Abu-Bakr, Sherifa M. organization: Chemistry Department of Natural and Microbial Products, National Research Centre – sequence: 3 givenname: Khaled H. surname: Hegab fullname: Hegab, Khaled H. organization: Department of Inorganic Chemistry and Pharmaceutical Research Department, Center of Excellence for Advanced Sciences, National Research Centre – sequence: 4 givenname: Wafaa surname: El-Eraky fullname: El-Eraky, Wafaa organization: Department of Pharmacology, National Research Centre – sequence: 5 givenname: Ahmed A. surname: El Beih fullname: El Beih, Ahmed A. organization: Chemistry Department of Natural and Microbial Products and Pharmaceutical Research Department, Center of Excellence for Advanced Sciences, National Research Centre – sequence: 6 givenname: Mohamed E. Abdel surname: Rehim fullname: Rehim, Mohamed E. Abdel organization: Department of Analytical Chemistry, Stockholm University |
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| Cites_doi | 10.1016/S0040-4020(01)80932-7 10.1002/jhet.5570350633 10.1016/0040-4020(95)00252-4 10.2298/JSC0607733N 10.1081/SIM-200059215 10.3998/ark.5550190.0008.e12 10.3181/00379727-111-27849 10.1080/10426500307892 10.1021/jm00394a025 10.1016/S0040-4020(02)00759-7 10.2478/v10007-010-0004-0 10.1016/j.bmc.2008.03.006 10.1070/RC1981v050n09ABEH002688 10.1016/j.ijfoodmicro.2007.07.064 10.1007/BF02716764 10.1055/s-1987-27946 10.1021/jm00192a015 10.1016/j.ejmech.2005.05.013 10.1080/10426500307886 10.1007/BF00471584 10.1128/AAC.40.1.234 10.1039/CO9970400373 10.1016/S0367-326X(03)00142-4 10.1016/S0277-5387(00)00404-6 10.1016/S1734-1140(09)70178-1 10.1021/ja01554a020 10.1016/S0040-4020(02)01023-2 10.1021/jm010041l 10.1016/j.ejmech.2005.05.005 |
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| Keywords | perimidine derivatives Quinoxaline derivatives Antiinflammatory activity Antimicrobial activity Mercapto-1 Transition metal complexes |
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| Snippet | New series of 1
H
-perimidine-2-thiol derivatives and (2-substituted-1
H
-perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C
24
H
14
N
4
S
2
O
2... New series of 1H-perimidine-2-thiol derivatives and (2-substituted-1H-perimidin-1-yl)ethane-1,2-dione derivatives and their ligands (C24H14N4S2O2) H2L1 and... |
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| SubjectTerms | Antiinflammatory activity Antimicrobial activity Catalysis Chemistry Chemistry and Materials Science Inorganic Chemistry Mercapto-1H-perimidine derivatives Physical Chemistry Quinoxaline derivatives Transition metal complexes |
| Title | Synthesis of new transition metal complexes of 1H-perimidine derivatives having antimicrobial and anti-inflammatory activities |
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