Low temperature seamless joining of SiC using a Ytterbium film

• Published in: Journal of the European Ceramic Society Vol. 41; no. 15; pp. 7507 - 7515
• Main Authors: Shi, Lin-Kun, Zhou, Xiaobing, Xu, Kai, Chang, Keke, Dai, Jian-Qing, Huang, Zhengren, Huang, Qing
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.12.2021
• Subjects: Electric field-assisted sintering; Joining; RE3Si2C2; SiC; Joining; SiC; RE3Si2C2; Electric field-assisted sintering
• ISSN: 0955-2219; 1873-619X
• DOI: 10.1016/j.jeurceramsoc.2021.08.057

Monolithic SiC, for the first time, was seamless joined at a low temperature of 1200 °C using electric field-assisted sintering technology. A 300 nm Yb coating on SiC was used as the joining filler to form Yb3Si2C2 via an in-situ reaction with the SiC. A liquid phase was formed by an eutectic reaction between Yb3Si2C2 and SiC. Almost completely seamless joints were formed by the precipitated SiC grains, which were fully consolidated with the SiC matrix with the help of in-situ formed liquid phase, followed by its elimination under the uniaxial pressure. The bending strength of the seamless joint joined at 1500 °C for 15 min was as high as 257.2 ± 31.1 MPa, which was comparable to the strength of the SiC matrix. As a result, the failure occurred in the matrix indicated a sound joint was obtained. The proposed low temperature seamless joining could potentially be used for joining of SiC-based composite.