Nanoindentation Stress Relaxation to Quantify Dislocation Velocity–Stress Exponent

• Published in: Crystals (Basel) Vol. 14; no. 8; p. 680
• Main Authors: Chang, Tzu-Yi, Vandenbroeder, Gavin, Frazer, David M., Yushu, Dewen, Pitts, Stephanie, Chen, Tianyi
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 01.08.2024; MDPI
• Subjects: activation volume; Aluminum; creep; Crystal dislocations; Dislocations in crystals; Experiments; Finite element analysis; MATERIALS SCIENCE; MATHEMATICS AND COMPUTING; Nanoindentation; nanomechanics; Nanotechnology; NUCLEAR FUEL CYCLE AND FUEL MATERIALS; Room temperature; scaling; Simulation; Strains and stresses; Stress relaxation; Stress relaxation (Materials); Stress relieving (Materials); Velocity; United States
• ISSN: 2073-4352; 2073-4352
• DOI: 10.3390/cryst14080680

This work reports a new methodology using indentation stress relaxation to characterize the dislocation velocity–stress exponent. Through the indentation stress relaxation process, the dislocation structure builds up at the rate governed by dislocation velocity, which is a function of the externally applied stress. The relationship between the dislocation velocity and stress can thus be derived from the indentation stress relaxation data of the stress as a function of time. In this study, instrumented nanoindentation stress relaxation experiments were performed on pure aluminum samples, following three different initial displacement rates of 100, 400, and 800 nm/s. Based on the scaling properties of dislocation kinetics, the data were interpreted to derive a dislocation velocity–stress exponent of 2.5 ± 0.5 for room-temperature aluminum. Crystal plasticity finite-element simulations were performed to illustrate the sensitivity of the proposed nanoindentation stress relaxation methodology to the dislocation velocity–stress exponent value.