Bonding Polycrystalline Zirconia With 10-MDP-containing Adhesives
The objective of this study was to evaluate the influence of adhesives with different 10-MDP concentrations on the shear bond strength of a resin cement to zirconia. Six experimental adhesives were prepared with the following composition: camphorquinone, 1,2-diaminobenzene, butylhydroxytoluene, diph...
Saved in:
Published in | Operative dentistry Vol. 42; no. 3; p. 335 |
---|---|
Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
United States
01.05.2017
|
Subjects | |
Online Access | Get more information |
Cover
Loading…
Summary: | The objective of this study was to evaluate the influence of adhesives with different 10-MDP concentrations on the shear bond strength of a resin cement to zirconia.
Six experimental adhesives were prepared with the following composition: camphorquinone, 1,2-diaminobenzene, butylhydroxytoluene, diphenyliodonium hexafluorophosphate, 2-hydroxyethyl methacrylate triethylene glycol dimethacrylate, ethoxylated bisphenol A glycol dimethacrylate, urethane dimethacrylate, bisphenol A diglycidyl methacrylate, and ethanol. The 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) monomer was added at 0wt%, 3wt%, 6wt%, 9wt%, 12wt%, or 15wt%. Three commercially available adhesives were evaluated: Single Bond Universal, Single Bond 2, and Signum Zirconia Bond. Resin cement cylinders made with RelyX Ultimate were bonded to yttria-stabilized tetragonal zirconia polycrystal with one of the evaluated adhesives and were subjected to the shear bond strength evaluation. Failure modes were analyzed with a stereoscopic loupe. Statistical analyses were performed with one-way analysis of variance and the Tukey's Honestly Significant Difference test (α=0.05). Pearson's was used to correlate the percentage of 10-MDP in the experimental adhesives and shear bond strength.
There were significant differences between adhesives (p<0.00001). The highest shear bond strength values were obtained with the Signum Zirconia Bond and Single Bond Universal. Single Bond 2 showed the lowest values. There were no differences between experimental adhesives. All groups showed adhesives failures. A nonlinear correlation was found between bond strength and percentage of 10-MDP in experimental adhesives (r=0.872).
The commercially available adhesives indicated for bonding to zirconia showed the highest bonding values. |
---|---|
ISSN: | 1559-2863 |
DOI: | 10.2341/16-156-L |