Strain-controlled cyclic stability and properties of Cu with highly oriented nanoscale twins

• Published in: Acta materialia Vol. 81; pp. 248 - 257
• Main Authors: PAN, Q. S, LU, L
• Format: Journal Article
• Language: English
• Published: Kidlington Elsevier 01.12.2014
• Subjects: Activation; Applied sciences; Channels; Copper; DISLOCATIONS; ELECTRODEPOSITION; Exact sciences and technology; Fatigue; Fatigue limit; FATIGUE PROPERTIES; GRAIN SIZE AND SHAPE; Low cycle fatigue; Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology; Metals. Metallurgy; MICROSTRUCTURES; Nanostructure; SOFTENING; Stability; STRAIN; TWINNING MECHANISMS; Cyclic stability; Cu; Stability; Nanoscale twins; Mechanical properties; Strain-controlled fatigue; Fatigue; Fatigue property
• ISSN: 1359-6454; 1873-2453
• DOI: 10.1016/j.actamat.2014.08.011

By means of a direct-current electrodeposition technique, bulk (3mm in thickness) polycrystalline Cu samples with preferentially oriented nanoscale twins have been synthesized. Strain-controlled pull-push fatigue tests of the nanotwinned Cu samples show that the cyclic stability is maintained after a short initially rapid cyclic hardening stage, distinct from continuous cyclic softening of ultrafine-grained Cu. The saturation stress increases with increasing strain amplitude and decreasing twin thickness, while the longer low cycle fatigue life is achieved at larger grain size. The strain-life and S-N curves reveal that the preferentially oriented nanotwins embedded in microsized grains enhance the low and high cycle fatigue property synergy for nanotwinned Cu, which has better low cycle fatigue life while maintaining higher endurance limit (90MPa at 107), compared with that of coarse-grained Cu and ultrafine-grained Cu. Besides the relatively stable microstructure, the activation of a single primary slip system, i.e. threading dislocation propagation inside nanoscale twin lamellar channels, dominates the steady state of nanotwinned samples.