Crystal structure of two polymorphs of molybdenyl salicylidene-2-furfuriliminate (HL1) [MoO2(L1)2]
The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO 2 (L 1 ) 2 ] have been solved by X-ray diffraction. Both complexes crystallize in centrosymmetric and non-centrosymmetric space groups ( P 2 1 / c and Р 2 1 , respectively) of monoclinic system and have simila...
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| Published in | Russian journal of inorganic chemistry Vol. 62; no. 7; pp. 900 - 904 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
01.07.2017
Springer Nature B.V |
| Subjects | |
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| Abstract | The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO
2
(L
1
)
2
] have been solved by X-ray diffraction. Both complexes crystallize in centrosymmetric and non-centrosymmetric space groups (
P
2
1
/
c
and
Р
2
1
, respectively) of monoclinic system and have similar structures and close geometric parameters. The Мо atoms have a distorted octahedral coordination to two terminal oxo ligands in
cis
-positions to each other and two pairs of the oxygen atoms (
cis
- to О(oxo)) and the nitrogen atoms (
trans
- to О(oxo)) of two bidentate chelate ligands (L
1
)
–
. |
|---|---|
| AbstractList | The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO
2
(L
1
)
2
] have been solved by X-ray diffraction. Both complexes crystallize in centrosymmetric and non-centrosymmetric space groups (
P
2
1
/
c
and
Р
2
1
, respectively) of monoclinic system and have similar structures and close geometric parameters. The Мо atoms have a distorted octahedral coordination to two terminal oxo ligands in
cis
-positions to each other and two pairs of the oxygen atoms (
cis
- to О(oxo)) and the nitrogen atoms (
trans
- to О(oxo)) of two bidentate chelate ligands (L
1
)
–
. The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO2(L1)2] have been solved by X-ray diffraction. Both complexes crystallize in centrosymmetric and non-centrosymmetric space groups (P21/c and Р21, respectively) of monoclinic system and have similar structures and close geometric parameters. The Мо atoms have a distorted octahedral coordination to two terminal oxo ligands in cis-positions to each other and two pairs of the oxygen atoms (cis- to О(oxo)) and the nitrogen atoms (trans- to О(oxo)) of two bidentate chelate ligands (L1)–. |
| Author | Sergienko, V. S. Abramenko, V. L. Gorbunova, Yu. E. |
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| References | ViossatB.RodierN.Acta Crystallogr., Sect. B1979352175 Porai-KoshitsM. A.AtovmyanL. O.Koord. Khim.1975112711:CAS:528:DyaE2MXmtVWnsrw%3D Porai-KoshitzM. A.Izv. Jugosl. Cent. Kristallogr. (Zagreb)1974919 ShustorovichE. M.Porai-KoshitsM. A.BuslaevYu. A.Coord. Chem. Rev.197511110.1016/S0010-8545(00)80300-8 SheldrickG. M.Acta Crystallogr., Sect. A19904646710.1107/S0108767390000277 TsucumaK.KawaguchiT.WatanabeT.Acta Crystallogr., Sect. B197531216510.1107/S0567740875007157 SergienkoV. S.Porai-KoshitsM. A.AbramenkoV. L.GarnovskiiA. D.Koord. Khim.19851113991:CAS:528:DyaL28Xislyntg%3D%3D AtovmyanL. O.SokolovaYu. A.Zh. Strukt. Khim.1971128511:CAS:528:DyaE38XjvVGmtA%3D%3D YamanouchiK.EnemarkJ. H.Inorg. Chem.19791816261:CAS:528:DyaE1MXktFahtLw%3D10.1021/ic50196a049 SergienkoV. S.AbramenkoV. L.GorbunovaYu. E.ChurakovA. V.Russ. J. Inorg. Chem. V.2017621751:CAS:528:DC%2BC2sXjtlGgt70%3D10.1134/S0036023617020152 SheldrickG. M.SHELXL-97: Program for the Refinment of Crystal Structure1997GöttingenUniv. of Göttingen V. S. Sergienko (1317_CR1) 2017; 62 G. M. Sheldrick (1317_CR3) 1997 M. A. Porai-Koshits (1317_CR5) 1975; 1 K. Yamanouchi (1317_CR10) 1979; 18 K. Tsucuma (1317_CR8) 1975; 31 V. S. Sergienko (1317_CR7) 1985; 11 G. M. Sheldrick (1317_CR2) 1990; 46 B. Viossat (1317_CR11) 1979; 35 M. A. Porai-Koshitz (1317_CR4) 1974; 9 E. M. Shustorovich (1317_CR6) 1975; 1 L. O. Atovmyan (1317_CR9) 1971; 12 |
| References_xml | – volume: 46 start-page: 467 year: 1990 ident: 1317_CR2 publication-title: Acta Crystallogr., Sect. A doi: 10.1107/S0108767390000277 contributor: fullname: G. M. Sheldrick – volume: 12 start-page: 851 year: 1971 ident: 1317_CR9 publication-title: Zh. Strukt. Khim. contributor: fullname: L. O. Atovmyan – volume: 11 start-page: 1399 year: 1985 ident: 1317_CR7 publication-title: Koord. Khim. contributor: fullname: V. S. Sergienko – volume: 1 start-page: 1 issue: 1 year: 1975 ident: 1317_CR6 publication-title: Coord. Chem. Rev. doi: 10.1016/S0010-8545(00)80300-8 contributor: fullname: E. M. Shustorovich – volume: 18 start-page: 1626 year: 1979 ident: 1317_CR10 publication-title: Inorg. Chem. doi: 10.1021/ic50196a049 contributor: fullname: K. Yamanouchi – volume: 62 start-page: 175 year: 2017 ident: 1317_CR1 publication-title: Russ. J. Inorg. Chem. V. doi: 10.1134/S0036023617020152 contributor: fullname: V. S. Sergienko – volume: 9 start-page: 19 year: 1974 ident: 1317_CR4 publication-title: Izv. Jugosl. Cent. Kristallogr. (Zagreb) contributor: fullname: M. A. Porai-Koshitz – volume: 35 start-page: 2175 year: 1979 ident: 1317_CR11 publication-title: Acta Crystallogr., Sect. B contributor: fullname: B. Viossat – volume-title: SHELXL-97: Program for the Refinment of Crystal Structure year: 1997 ident: 1317_CR3 contributor: fullname: G. M. Sheldrick – volume: 1 start-page: 1271 year: 1975 ident: 1317_CR5 publication-title: Koord. Khim. contributor: fullname: M. A. Porai-Koshits – volume: 31 start-page: 2165 year: 1975 ident: 1317_CR8 publication-title: Acta Crystallogr., Sect. B doi: 10.1107/S0567740875007157 contributor: fullname: K. Tsucuma |
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| Snippet | The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO
2
(L
1
)
2
] have been solved by X-ray diffraction. Both complexes... The crystal structures of two polymorphs of molybdenyl salicylidene-2-furfuryliminate [MoO2(L1)2] have been solved by X-ray diffraction. Both complexes... |
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| SubjectTerms | Atomic structure Chemistry Chemistry and Materials Science Coordination Compounds Crystal structure Diffraction Distortion Inorganic Chemistry Ligands Nitrogen atoms Oxygen atoms X-ray diffraction X-rays |
| Title | Crystal structure of two polymorphs of molybdenyl salicylidene-2-furfuriliminate (HL1) [MoO2(L1)2] |
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