Synthesis, Molecular, and Crystal Structure of Tris(2-carbamoylmethoxyphenyl)phosphine Oxide

New tripodal ligand, tris(2-carbamoylmethoxyphenyl)phosphine oxide, has been synthesized via the alkylation of tris(2-hydroxyphenyl)phosphine oxide with chloroacetamide. The ligand structure has been studied by means of IR and NMR ( 1 H, 31 P) spectroscopy as well as X-ray diffraction.

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Bibliographic Details
Published inRussian journal of general chemistry Vol. 90; no. 10; pp. 1840 - 1844
Main Authors Baulina, T. V., Kudryavtsev, I. Yu, Artem’ev, A. V., Bagryanskaya, I. Yu, Pasechnik, M. P., Brel, V. K.
Format Journal Article
LanguageEnglish
Published Moscow Pleiades Publishing 01.10.2020
Springer Nature
Springer Nature B.V
Subjects
Alkylation
Chemical synthesis
Chemistry
Chemistry and Materials Science
Chemistry, Multidisciplinary
Chemistry/Food Science
Crystal structure
Crystals
Infrared spectroscopy
Ligands
Molecular structure
NMR
Nuclear magnetic resonance
Phosphine oxide
Physical Sciences
Science & Technology
crystal and molecular structure
tripodal ligand
tris(2-carbamoylmethoxyphenyl)phosphine oxide
PLATFORM
EXTRACTION
COORDINATION PROPERTIES
LIGANDS
NITRATE
RECEPTORS
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Summary:New tripodal ligand, tris(2-carbamoylmethoxyphenyl)phosphine oxide, has been synthesized via the alkylation of tris(2-hydroxyphenyl)phosphine oxide with chloroacetamide. The ligand structure has been studied by means of IR and NMR ( 1 H, 31 P) spectroscopy as well as X-ray diffraction.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363220100059