Rhodium-catalyzed C-H activation/cyclization of aryl sulfoximines with iodonium ylides towards polycyclic 1,2-benzothiazines

The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed for the first time. In this report, C-H and N-H bond functionalization was realized towards a series of tricyclic and tetracyclic sulfoximine...

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Published inOrganic & biomolecular chemistry Vol. 19; no. 46; pp. 185 - 189
Main Authors Huang, Gao, Shan, Yujia, Yu, Jin-Tao, Pan, Changduo
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 01.12.2021
Royal Society of Chemistry
Subjects
Aromatic compounds
Catalysis
Chemistry
Chemistry, Organic
Hydrogen bonds
Physical Sciences
Rhodium
Science & Technology
FUNCTIONALIZATION
KETONES
ACTIVATION
INSERTION
OXIDATIVE ANNULATION
INDOLES
ACCESS
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Abstract The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed for the first time. In this report, C-H and N-H bond functionalization was realized towards a series of tricyclic and tetracyclic sulfoximine derivatives with moderate to excellent yields under simple reaction conditions. The synthesis of polycyclic 1,2-benzothiazines through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides has been developed for the first time.
AbstractList The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C–H activation/cyclization of S-aryl sulfoximines with iodonium ylides was developed for the first time. In this report, C–H and N–H bond functionalization was realized towards a series of tricyclic and tetracyclic sulfoximine derivatives with moderate to excellent yields under simple reaction conditions.
The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C–H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed for the first time. In this report, C–H and N–H bond functionalization was realized towards a series of tricyclic and tetracyclic sulfoximine derivatives with moderate to excellent yields under simple reaction conditions.
The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed for the first time. In this report, C-H and N-H bond functionalization was realized towards a series of tricyclic and tetracyclic sulfoximine derivatives with moderate to excellent yields under simple reaction conditions. The synthesis of polycyclic 1,2-benzothiazines through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides has been developed for the first time.
Author Huang, Gao
Shan, Yujia
Pan, Changduo
Yu, Jin-Tao
AuthorAffiliation School of Petrochemical Engineering
Jiangsu University of Technology
School of Chemical and Environmental Engineering
Jiangsu Key Laboratory of Advanced Catalytic Materials & Technology
Changzhou University
AuthorAffiliation_xml – name: School of Chemical and Environmental Engineering
– name: Jiangsu University of Technology
– name: School of Petrochemical Engineering
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– name: Changzhou University
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  surname: Huang
  fullname: Huang, Gao
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  givenname: Yujia
  surname: Shan
  fullname: Shan, Yujia
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  givenname: Jin-Tao
  surname: Yu
  fullname: Yu, Jin-Tao
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  givenname: Changduo
  surname: Pan
  fullname: Pan, Changduo
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KETONES
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OXIDATIVE ANNULATION
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Snippet The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C-H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed...
The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C-H activation/cyclization of S-aryl sulfoximines with iodonium ylides was developed...
The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C–H activation/cyclization of S -aryl sulfoximines with iodonium ylides was developed...
The synthesis of 1,2-benzothiazine derivatives through rhodium-catalyzed C–H activation/cyclization of S-aryl sulfoximines with iodonium ylides was developed...
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SubjectTerms Aromatic compounds
Catalysis
Chemistry
Chemistry, Organic
Hydrogen bonds
Physical Sciences
Rhodium
Science & Technology
Title Rhodium-catalyzed C-H activation/cyclization of aryl sulfoximines with iodonium ylides towards polycyclic 1,2-benzothiazines
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