Nonlinear model predictive control of crystal size in batch cooling crystallization processes

• Published in: Journal of process control Vol. 128; p. 103020
• Main Authors: Wang, Liangyong, Zhu, Yaolong, Gan, Chenyang
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.08.2023
• Subjects: Cooling crystallization; Crystal size; Deep learning; Image analysis; Nonlinear model predictive control; Path following control; Deep learning; Crystal size; Image analysis; Nonlinear model predictive control; Cooling crystallization; Path following control
• ISSN: 0959-1524; 1873-2771
• DOI: 10.1016/j.jprocont.2023.103020

The paper proposes a model-based nonlinear model predictive control (NMPC) method for online control of crystal mean size and standard deviation in cooling crystallization process. Image analysis method using deep learning neural network and mathematical statistical method are performed to obtain the mean size and standard deviation of crystal population. The nonlinear prediction model for the NMPC is derived from the input and output data. The effectiveness of the proposed NMPC method is evaluated by the alum cooling crystallization experiments. Experimental results demonstrate the benefits of the proposed combination of image analysis and feedback control of the crystal mean size and standard deviation. The control performance of NMPC is superior to model-free path following control (PFC) method due to the prediction and optimization capabilities of NMPC. •Model-based nonlinear model predictive control for crystal mean size and standard deviation.•Model-free path following control for crystal mean size and standard deviation.•Image analysis method using deep learning to obtain pixel-level instance segmentation.•The effectiveness of the proposed control methods is evaluated by the alum cooling crystallization experiments.