Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO2 nanostructures

The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy...

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Published inInternational journal of materials research Vol. 109; no. 4; pp. 362 - 365
Main Authors Tian, Pei, Lin, Hechun
Format Journal Article
LanguageEnglish
Published De Gruyter 01.04.2018
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ISSN1862-5282
2195-8556
DOI10.3139/146.111606

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Abstract The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO nanostructures.
AbstractList The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO nanostructures.
The [Zr(OH) 5 ] − imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO 2 by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO 2 nanostructures.
Author Lin, Hechun
Tian, Pei
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Snippet The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was...
The [Zr(OH) 5 ] − imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which...
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StartPage 362
SubjectTerms Anion exchange reaction
Ionic liquid
Nanoplate
Zirconia precursor
Zirconium oxide
Title Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO2 nanostructures
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