Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO2 nanostructures
The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy...
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Published in | International journal of materials research Vol. 109; no. 4; pp. 362 - 365 |
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Main Authors | , |
Format | Journal Article |
Language | English |
Published |
De Gruyter
01.04.2018
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Subjects | |
Online Access | Get full text |
ISSN | 1862-5282 2195-8556 |
DOI | 10.3139/146.111606 |
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Abstract | The [Zr(OH)
imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO
by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO
nanostructures. |
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AbstractList | The [Zr(OH)
imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO
by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO
nanostructures. The [Zr(OH) 5 ] − imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO 2 by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO 2 nanostructures. |
Author | Lin, Hechun Tian, Pei |
Author_xml | – sequence: 1 givenname: Pei surname: Tian fullname: Tian, Pei organization: Key Laboratory of Polar Materials and Devices, Ministry of Education, East China Normal University, Shanghai, P. R. China – sequence: 2 givenname: Hechun surname: Lin fullname: Lin, Hechun organization: Key Laboratory of Polar Materials and Devices, Ministry of Education, East China Normal University, Shanghai, P. R. China |
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Cites_doi | 10.1039/B801395K 10.1016/j.jcis.2009.02.025 10.1002/anie.200460091 10.1016/j.ica.2016.03.023 10.1039/C4CC02021A 10.1002/9783527621194 10.1021/cm101490w 10.1039/C4NJ00152D 10.1016/S0022-3697(99)00221-8 10.1039/C3CE41203B 10.1016/j.jssc.2017.01.008 10.1021/cr078399y 10.1039/C4CE00987H 10.1002/zaac.201000073 10.1021/jp9077135 |
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Snippet | The [Zr(OH)
imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was... The [Zr(OH) 5 ] − imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which... |
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StartPage | 362 |
SubjectTerms | Anion exchange reaction Ionic liquid Nanoplate Zirconia precursor Zirconium oxide |
Title | Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO2 nanostructures |
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