Formation of zirconia precursor nanoplates mediated by ionic liquid and transformation to monoclinic ZrO2 nanostructures

The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy...

Full description

Saved in:
Bibliographic Details
Published inInternational journal of materials research Vol. 109; no. 4; pp. 362 - 365
Main Authors Tian, Pei, Lin, Hechun
Format Journal Article
LanguageEnglish
Published De Gruyter 01.04.2018
Subjects
Anion exchange reaction
Ionic liquid
Nanoplate
Zirconia precursor
Zirconium oxide
Online AccessGet full text

Cover

More Information
Summary:The [Zr(OH) imidazolium complex was used to synthesize a zirconia precursor with plate-like nanostructue hydrolyzed under strong acid conditions, which was characterized by means of powder X-ray diffraction, thermogravimetric-differential scanning calorimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, elemental analysis, inductively coupled plasma and electronic differential system. The zirconia precursor can be transformed to monoclinic ZrO by annealing at a temperature above 400 °C. With the increasing of the curing temperature, it tended to give rise to porous ZrO nanostructures.
ISSN:1862-5282
2195-8556
DOI:10.3139/146.111606