On the evolution of a deformation induced nanostructure in a Ni3Al alloy

• Published in: Acta materialia Vol. 53; no. 10; pp. 3031 - 3040
• Main Authors: RENTENBERGER, C, KARNTHALER, H. P
• Format: Journal Article
• Language: English
• Published: Oxford Elsevier Science 01.06.2005
• Subjects: Applied sciences; Exact sciences and technology; Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology; Metals. Metallurgy; Nickel base alloys; Severe plastic deformation; Transmission electron microscopy; Intermetallic compound; Nickel aluminide; Geometrically necessary dislocations; Mechanical properties; Nickel Aluminides; Nanostructure; Aluminium alloy; Plastic deformation; Dislocation
• ISSN: 1359-6454; 1873-2453
• DOI: 10.1016/j.actamat.2005.03.016

The evolution of a nanocrystalline structure of a polycrystalline L12 ordered Ni3Al alloy was investigated by transmission electron microscopy methods after severe plastic deformation by high pressure torsion. As a precursor of the nanocrystalline structure, blocks and bands are formed containing misoriented fragments in the 100 nm range separated by a three-dimensional array of low angle boundaries. The inhomogeneous deformation leads to localized disorder and a high density of dislocations, especially geometrically necessary ones. Dynamic recovery causes a heterogeneous formation of the nanocrystalline structure. The interplay of dynamic recovery and disordering yields nanograins in the disordered state. At strains of about 8000% a duplex structure is formed consisting of veins of disordered nanograins that are embedded in the ordered coarse-grained structure. The nanocrystalline veins showing a weak texture grow by the formation of nanograins generated autocatalytically at their interface. Finally, at strains above 50,000% the whole volume transforms to the nanocrystalline structure.