Chloropolyfluoro-derivatives of ethyl methyl ether

Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl 2-UV and CHC...

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Published inJournal of fluorine chemistry Vol. 82; no. 1; pp. 9 - 12
Main Authors Coe, Paul L., Rowbotham, Roger A., Tatlow, John Colin
Format Journal Article
LanguageEnglish
Published LAUSANNE Elsevier B.V 01.04.1997
Elsevier
Subjects
Chemistry
Chemistry, Inorganic & Nuclear
Chemistry, Organic
Chloropolyfluoro(ethyl methyl) ethers
Physical Sciences
Potassium tetrafluorocobaltate fluorination
Science & Technology
Potassium tetrafluorocobaltate fluorination
Chloropolyfluoro(ethyl methyl) ethers
potassium tetrafluorocobaltate fluorination
DEHYDROFLUORINATION
chloropolyfluoro(ethylmethyl) ethers
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Abstract Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl 2-UV and CHClFCHFOCHF 2 gave halogeno-ethers by exchange of Cl for both H and also F.
AbstractList Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180-250 degrees C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectrescopically. Cl-2-UV and CHClFCHFOCHF2 gave halogeno-ethers by exchange of Cl for both H and also F. (C) 1997 Elsevier Science S.A. All rights reserved.
Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl 2-UV and CHClFCHFOCHF 2 gave halogeno-ethers by exchange of Cl for both H and also F.
Author Coe, Paul L.
Tatlow, John Colin
Rowbotham, Roger A.
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Issue 1
Keywords Potassium tetrafluorocobaltate fluorination
Chloropolyfluoro(ethyl methyl) ethers
potassium tetrafluorocobaltate fluorination
DEHYDROFLUORINATION
chloropolyfluoro(ethylmethyl) ethers
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References Coe, Lennard, Tatlow (bib4) 1996; 80
OCHCl
Burdon, Coe, Smith, Tatlow (bib5) 1991; 52
OH with SOCl
made by reaction of MeOCH
MeOH (base) ⇒ CHClFCF
was used.
HF/SbCl
Forche (bib6) 1962; Band V/3
who made these products by electrochemical fluorination of chloride-containing ethers.
on CHClFCF
Bailey, Plevey, Tatlow (bib8) 1987; 37
OMe.
Tatlow (bib1) 1995; 75
CH
in the present work PCl
this preparation was by the action of CoF
.
Brandwood, Coe, Ely, Tatlow (bib2) 1975; 5
CHC1FCF
route CClF=CF
OCHF
Brandwood, Coe, Tatlow (bib3) 1975; 6
OMe + Cl
CHClFCF
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  ident: 10.1016/S0022-1139(96)03549-X_bib7_3
  publication-title: J. Am. Chem. Soc.
  doi: 10.1021/ja01629a124
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Snippet Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl...
Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180-250 degrees C gave various tri-, tetra-, penta- and...
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elsevier
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SubjectTerms Chemistry
Chemistry, Inorganic & Nuclear
Chemistry, Organic
Chloropolyfluoro(ethyl methyl) ethers
Physical Sciences
Potassium tetrafluorocobaltate fluorination
Science & Technology
Title Chloropolyfluoro-derivatives of ethyl methyl ether
URI https://dx.doi.org/10.1016/S0022-1139(96)03549-X
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