Chloropolyfluoro-derivatives of ethyl methyl ether
Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl 2-UV and CHC...
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Published in | Journal of fluorine chemistry Vol. 82; no. 1; pp. 9 - 12 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
LAUSANNE
Elsevier B.V
01.04.1997
Elsevier |
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Abstract | Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl
2-UV and CHClFCHFOCHF
2 gave halogeno-ethers by exchange of Cl for both H and also F. |
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AbstractList | Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180-250 degrees C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectrescopically. Cl-2-UV and CHClFCHFOCHF2 gave halogeno-ethers by exchange of Cl for both H and also F. (C) 1997 Elsevier Science S.A. All rights reserved. Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl methyl) ethers. Cobalt trifluoride afforded the same products in poorer recoveries. Structures were established spectroscopically. Cl 2-UV and CHClFCHFOCHF 2 gave halogeno-ethers by exchange of Cl for both H and also F. |
Author | Coe, Paul L. Tatlow, John Colin Rowbotham, Roger A. |
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Cites_doi | 10.1016/S0022-1139(00)81733-9 10.1016/S0022-1139(96)03501-4 10.1021/ja01629a123 10.1016/S0022-1139(00)80133-5 10.1021/jm00288a014 10.1016/S0022-1139(00)85288-4 10.1016/0022-1139(95)03293-M 10.1016/S0022-1139(00)81654-1 10.1039/jr9650007370 10.1021/ja01623a045 10.1021/jm00276a008 10.1016/S0022-1139(00)83080-8 10.1021/ja01629a124 10.1039/JR9290000268 |
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Keywords | Potassium tetrafluorocobaltate fluorination Chloropolyfluoro(ethyl methyl) ethers potassium tetrafluorocobaltate fluorination DEHYDROFLUORINATION chloropolyfluoro(ethylmethyl) ethers |
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Snippet | Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180–250 °C gave various tri-, tetra-, penta- and hexafluoro(2-chloroethyl... Fluorination of 2-chloroethyl methyl ether by potassium tetrafluorocobaltate at 180-250 degrees C gave various tri-, tetra-, penta- and... |
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SubjectTerms | Chemistry Chemistry, Inorganic & Nuclear Chemistry, Organic Chloropolyfluoro(ethyl methyl) ethers Physical Sciences Potassium tetrafluorocobaltate fluorination Science & Technology |
Title | Chloropolyfluoro-derivatives of ethyl methyl ether |
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