Synthesis of 1,5-benzothiazepines with microwave irradiation under solvent and catalyst-free conditions

Microwave irradiation of alpha,beta-unsaturated ketones (chalcones) and o-aminothiophenol in the absence of solvent and catalyst provides a highly efficient methodology for the synthesis of 1,5-benzothiazepines in moderate to good yields.

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Bibliographic Details
Published inJournal of chemical research Vol. 2009; no. 3; pp. 178 - 179
Main Authors Rahman, M., Roy, A., Majee, A., Hajra, A.
Format Journal Article
LanguageEnglish
Published LONDON Sage 01.03.2009
Sage Publications Ltd
Subjects
Catalysts
Chemistry
Chemistry, Multidisciplinary
Irradiation
Ketones
Methodology
Microwaves
Physical Sciences
Science & Technology
Solvents
Synthesis
ASSISTED SYNTHESIS
CARBONYL COMPOUND
SUBSTITUTED PYRROLES
alpha,beta-unsaturated ketone
HIGHLY EFFICIENT
ALCOHOLS
THIOLS
AMINES
SURFACE
CONDENSATION
o-aminothiophenol
DERIVATIVES
microwave
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Summary:Microwave irradiation of alpha,beta-unsaturated ketones (chalcones) and o-aminothiophenol in the absence of solvent and catalyst provides a highly efficient methodology for the synthesis of 1,5-benzothiazepines in moderate to good yields.
Bibliography:ObjectType-Article-2
SourceType-Scholarly Journals-1
ObjectType-Feature-1
content type line 23
ISSN:1747-5198
2047-6507
DOI:10.3184/030823409X416965