One-Pot Amide Synthesis via Thermal Decomposition N-Acylureas under Microwave Irradiation

A simple one-pot amidation of carboxylic acids promoted by microwave irradiation is described. Reaction includes formation N-acylureas via interaction carboxylic acids and N,N-dicyclohexylcarbodiimide followed thermal decomposition N-acylureas in microwave reactor. This method allows carrying out th...

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Bibliographic Details
Published inKey Engineering Materials Vol. 685; pp. 785 - 788
Main Authors Sarycheva, T.A., Soldatova, N.S., Orlova, K.V.
Format Journal Article
LanguageEnglish
Published Zurich Trans Tech Publications Ltd 01.02.2016
Subjects
Amides
Carboxylic acids
Formations
Irradiation
Microwaves
Reactors
Synthesis
Thermal decomposition
N-Acylureas
Microwave Irradiation
Amidation
Carbodiimides
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Summary:A simple one-pot amidation of carboxylic acids promoted by microwave irradiation is described. Reaction includes formation N-acylureas via interaction carboxylic acids and N,N-dicyclohexylcarbodiimide followed thermal decomposition N-acylureas in microwave reactor. This method allows carrying out the reaction in a short time with good yields.
Bibliography:Selected, peer reviewed papers from the IV International Conference for Young Scientists “High Technology: Research and Applications 2015” (HTRA 2015), April 21-24, 2015, Tomsk, Russia
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ISBN:3038357081
9783038357087
ISSN:1013-9826
1662-9795
1662-9795
DOI:10.4028/www.scientific.net/KEM.685.785