Hot-injection synthesis of iron/iron oxide core/shell nanoparticles for T2 contrast enhancement in magnetic resonance imaging
Here we report a new, bench-top synthesis for iron/iron oxide core/shell nanoparticles via the thermal decomposition of Fe(η(5)-C(6)H(3)Me(4))(2). The iron/iron oxide core/shell nanoparticles are superparamagnetic at room temperature and show improved negative contrast in T(2)-weighted MR imaging co...
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| Published in | Chemical communications (Cambridge, England) Vol. 47; no. 32; pp. 9221 - 9223 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
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28.08.2011
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| Abstract | Here we report a new, bench-top synthesis for iron/iron oxide core/shell nanoparticles via the thermal decomposition of Fe(η(5)-C(6)H(3)Me(4))(2). The iron/iron oxide core/shell nanoparticles are superparamagnetic at room temperature and show improved negative contrast in T(2)-weighted MR imaging compared to pure iron oxides nanoparticles, and have a transverse relaxivity (r(2)) of 332 mM(-1) s(-1). |
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| AbstractList | Here we report a new, bench-top synthesis for iron/iron oxide core/shell nanoparticles via the thermal decomposition of Fe([small eta]5-C6H3Me4)2. The iron/iron oxide core/shell nanoparticles are superparamagnetic at room temperature and show improved negative contrast in T2-weighted MR imaging compared to pure iron oxides nanoparticles, and have a transverse relaxivity (r2) of 332 mM-1 s-1. Here we report a new, bench-top synthesis for iron/iron oxide core/shell nanoparticles via the thermal decomposition of Fe(η(5)-C(6)H(3)Me(4))(2). The iron/iron oxide core/shell nanoparticles are superparamagnetic at room temperature and show improved negative contrast in T(2)-weighted MR imaging compared to pure iron oxides nanoparticles, and have a transverse relaxivity (r(2)) of 332 mM(-1) s(-1). |
| Author | Ferguson, Peter Spencer, John L Prabakar, Sujay Lendrum, Conrad D Tilley, Richard D Ruck, Ben J Allan, Kathryn M Cheong, Soshan Hermans, Ian F Herman, David A J |
| Author_xml | – sequence: 1 givenname: David A J surname: Herman fullname: Herman, David A J organization: School of Chemical and Physical Sciences and The MacDiarmid Institute of Advanced Materials and Nanotechnology, Victoria University of Wellington, P.O. Box 600, Wellington, New Zealand – sequence: 2 givenname: Peter surname: Ferguson fullname: Ferguson, Peter – sequence: 3 givenname: Soshan surname: Cheong fullname: Cheong, Soshan – sequence: 4 givenname: Ian F surname: Hermans fullname: Hermans, Ian F – sequence: 5 givenname: Ben J surname: Ruck fullname: Ruck, Ben J – sequence: 6 givenname: Kathryn M surname: Allan fullname: Allan, Kathryn M – sequence: 7 givenname: Sujay surname: Prabakar fullname: Prabakar, Sujay – sequence: 8 givenname: John L surname: Spencer fullname: Spencer, John L – sequence: 9 givenname: Conrad D surname: Lendrum fullname: Lendrum, Conrad D – sequence: 10 givenname: Richard D surname: Tilley fullname: Tilley, Richard D |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/21761066$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | Contrast Media - chemical synthesis Contrast Media - chemistry Ferric Compounds - chemical synthesis Ferric Compounds - chemistry Hot Temperature Imaging Iron Iron oxides Magnetic resonance imaging Magnetic Resonance Imaging - methods Nanoparticles Nanoparticles - chemistry Nanoparticles - ultrastructure Nanotechnology - methods Shells Synthesis Thermal decomposition |
| Title | Hot-injection synthesis of iron/iron oxide core/shell nanoparticles for T2 contrast enhancement in magnetic resonance imaging |
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