Solvothermal synthesis and characterizations of monophenyltin complexes in drum conformations

A series of drum structures of organotin complexes with various carboxylic acids have been solvothermally synthesized and characterized. The molecular structure analyses reveal that all of the complexes have endo drum structures. A series of drum structures of organotin complexes with various carbox...

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Published inPolyhedron Vol. 29; no. 2; pp. 881 - 885
Main Authors Ma, Chun-Lin, Ren, Yun, Wang, Yue-Rong, Zhang, Ru-Fen
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.02.2010
Subjects
Carboxylic acids
Drum structures
Organotin
Solvothermal synthesis
Drum structures
Carboxylic acids
Organotin
Solvothermal synthesis
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Summary:A series of drum structures of organotin complexes with various carboxylic acids have been solvothermally synthesized and characterized. The molecular structure analyses reveal that all of the complexes have endo drum structures. A series of drum structures of organotin complexes with various carboxylic acids have been solvothermally synthesized and characterized by elemental analysis, FT-IR, NMR ( 1H, 13C and 119Sn) spectra and X-ray crystallography. The molecular structure analyses reveal that all of the complexes have endo drum structures. Furthermore, each of the drum structures has a hole, in which atoms of a given radius could be held.
ISSN:0277-5387
DOI:10.1016/j.poly.2009.10.013