Synthesis, crystal structures and biological activities of palladium(II) complexes of benzimidazole and 2-methylbenzimidazole

Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and the crystal structures of two of them, [Pd(benzimidazole)2Br2]·2DMSO (1) and [Pd(2-methylbenzimidazole)2I2] (5) were determined by X-ray crystallography. In both complexes, the palladium(II) ion is boun...

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Published inPolyhedron Vol. 170; pp. 537 - 543
Main Authors Sadaf, Haseeba, Imtiaz-ud-Din, Fettouhi, Mohammed, Fazal, Atif, Ahmad, Saeed, Farooqi, Bilal Ahmad, Nadeem, Shafqat, Ihsan-ul-Haq, Ahmad, Waqar
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 15.09.2019
Subjects
2-Methylbenzimidazole
Benzimidazole
Biological activity
Palladium(II)
X-ray structure
Palladium(II)
X-ray structure
Benzimidazole
2-Methylbenzimidazole
Biological activity
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Abstract Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and the crystal structures of two of them, [Pd(benzimidazole)2Br2]·2DMSO (1) and [Pd(2-methylbenzimidazole)2I2] (5) were determined by X-ray crystallography. In both complexes, the palladium(II) ion is bound to two nitrogen atoms of benzimidazoles and two halide ions at trans positions, adopting a nearly regular square planar geometry. The complexes exhibited moderate antimicrobial activities but their antidiabetic properties were momentous with respect to the standard drug. [Display omitted] Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and characterized by thermal analysis and, IR and NMR spectroscopy. The crystal structures of two of them, trans-[Pd(benzimidazole)2Br2]·2DMSO (1) and trans-[Pd(2-methylbenzimidazole)2I2] (5) were determined by X-ray crystallography, which describe a square planar coordination environment around the Pd(II) ions. Compound 1 crystallizes as a DMSO solvate. The solid state structures of both complexes are stabilized by hydrogen bonding interactions. The biological evaluation of the complexes showed that they exhibited moderate antimicrobial activities but their antidiabetic properties were momentous with respect to the standard drug.
AbstractList Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and the crystal structures of two of them, [Pd(benzimidazole)2Br2]·2DMSO (1) and [Pd(2-methylbenzimidazole)2I2] (5) were determined by X-ray crystallography. In both complexes, the palladium(II) ion is bound to two nitrogen atoms of benzimidazoles and two halide ions at trans positions, adopting a nearly regular square planar geometry. The complexes exhibited moderate antimicrobial activities but their antidiabetic properties were momentous with respect to the standard drug. [Display omitted] Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and characterized by thermal analysis and, IR and NMR spectroscopy. The crystal structures of two of them, trans-[Pd(benzimidazole)2Br2]·2DMSO (1) and trans-[Pd(2-methylbenzimidazole)2I2] (5) were determined by X-ray crystallography, which describe a square planar coordination environment around the Pd(II) ions. Compound 1 crystallizes as a DMSO solvate. The solid state structures of both complexes are stabilized by hydrogen bonding interactions. The biological evaluation of the complexes showed that they exhibited moderate antimicrobial activities but their antidiabetic properties were momentous with respect to the standard drug.
Author Ahmad, Saeed
Imtiaz-ud-Din
Farooqi, Bilal Ahmad
Sadaf, Haseeba
Fazal, Atif
Ihsan-ul-Haq
Ahmad, Waqar
Fettouhi, Mohammed
Nadeem, Shafqat
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Keywords Palladium(II)
X-ray structure
Benzimidazole
2-Methylbenzimidazole
Biological activity
Language English
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Snippet Five palladium(II) complexes (1–5) with benzimidazole and 2-methylbenzimidazole were prepared and the crystal structures of two of them,...
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StartPage 537
SubjectTerms 2-Methylbenzimidazole
Benzimidazole
Biological activity
Palladium(II)
X-ray structure
Title Synthesis, crystal structures and biological activities of palladium(II) complexes of benzimidazole and 2-methylbenzimidazole
URI https://dx.doi.org/10.1016/j.poly.2019.06.025
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