Preparation, heat treatment and photoluminescence properties of V-doped ZnO–SiO2–B2O3 glasses
Four glasses in ZnO–SiO2–B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV region of zinc borosilicate glasses used in superfast scintillators. The effect of vanadium addition and heat treatment on phase formation, mic...
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Published in | Journal of luminescence Vol. 132; no. 5; pp. 1126 - 1132 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.05.2012
Elsevier |
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Abstract | Four glasses in ZnO–SiO2–B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV region of zinc borosilicate glasses used in superfast scintillators. The effect of vanadium addition and heat treatment on phase formation, microstructure and photoluminescence properties of the glasses was characterized by means of DTA, XRD, SEM and fluorescence spectrophotometer. Vanadium contributed to the near-band-edge emission in two ways, by introducing donor levels in the energy band of ZnO particles and by facilitating the precipitation of ZnO and willemite crystals. Furthermore, nucleation of willemite and zinc oxide phases, which are both the origins of the intense emission bands in the UV region, was facilitated with increasing either the time or temperature of heat treatments. Photoluminescence spectra showed the elimination of the visible emission band which is favorable in scintillating glasses.
► Phase analysis, thermal behavior, microstructure and photoluminescence properties. ► Crystallization driving forces and mechanisms. ► Optical basicity of ZnO–SiO2–B2O3 glasses. |
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AbstractList | Four glasses in ZnO–SiO2–B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV region of zinc borosilicate glasses used in superfast scintillators. The effect of vanadium addition and heat treatment on phase formation, microstructure and photoluminescence properties of the glasses was characterized by means of DTA, XRD, SEM and fluorescence spectrophotometer. Vanadium contributed to the near-band-edge emission in two ways, by introducing donor levels in the energy band of ZnO particles and by facilitating the precipitation of ZnO and willemite crystals. Furthermore, nucleation of willemite and zinc oxide phases, which are both the origins of the intense emission bands in the UV region, was facilitated with increasing either the time or temperature of heat treatments. Photoluminescence spectra showed the elimination of the visible emission band which is favorable in scintillating glasses.
► Phase analysis, thermal behavior, microstructure and photoluminescence properties. ► Crystallization driving forces and mechanisms. ► Optical basicity of ZnO–SiO2–B2O3 glasses. Four glasses in ZnO-SiO2-B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV region of zinc borosilicate glasses used in superfast scintillators. The effect of vanadium addition and heat treatment on phase formation, microstructure and photoluminescence properties of the glasses was characterized by means of DTA, XRD, SEM and fluorescence spectrophotometer. Vanadium contributed to the near-band-edge emission in two ways, by introducing donor levels in the energy band of ZnO particles and by facilitating the precipitation of ZnO and willemite crystals. Furthermore, nucleation of willemite and zinc oxide phases, which are both the origins of the intense emission bands in the UV region, was facilitated with increasing either the time or temperature of heat treatments. Photoluminescence spectra showed the elimination of the visible emission band which is favorable in scintillating glasses. |
Author | Hamnabard, Zohreh Maghsoudipour, Amir Baghshahi, Saeid Khalkhali, Zahra Qazvini, Shamsi Sadat Alavi |
Author_xml | – sequence: 1 givenname: Zohreh surname: Hamnabard fullname: Hamnabard, Zohreh email: zhamnabard@nrcam.org organization: Materials Research School, Ceramic Group, P.O. Box 14395-836, Alborz, Iran – sequence: 2 givenname: Zahra surname: Khalkhali fullname: Khalkhali, Zahra email: khalkhali_z@yahoo.com organization: Department of Material Science, Ceramic Division, Iran University of Science and Technology, Tehran, Iran – sequence: 3 givenname: Shamsi Sadat Alavi surname: Qazvini fullname: Qazvini, Shamsi Sadat Alavi email: IRUH81@yahoo.com organization: Faculty of Materials Engineering, Science and Research Branch, Islamic Azad University, Tehran, Iran – sequence: 4 givenname: Saeid surname: Baghshahi fullname: Baghshahi, Saeid email: s.baghshahi@ikiu.ac.ir organization: Faculty of Engineering and Technology, I.K.I. University, Qazvin, Iran – sequence: 5 givenname: Amir surname: Maghsoudipour fullname: Maghsoudipour, Amir email: a_maghsoudi@merc.ac.ir organization: Ceramic Division, Materials and Energy Research Center, Alborz, Iran |
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Keywords | Borosilicate glass Near band edge emission ZnO-based scintilator Vanadium Photoluminescence Scanning electron microscopy Impurity density Ternary systems Fluorescence Liquid state quenching Differential thermal analysis XRD Heat treatments Vanadium additions Ultraviolet radiation Scintillator Zinc oxide Donor center Microstructure |
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Snippet | Four glasses in ZnO–SiO2–B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV... Four glasses in ZnO-SiO2-B2O3 ternary system were prepared by the melt quenching method with the objective of optimizing sub-nanosecond emission over the UV... |
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SubjectTerms | Amorphous materials, glasses and other disordered solids Borosilicate glass Borosilicate glasses Condensed matter: electronic structure, electrical, magnetic, and optical properties Emission Exact sciences and technology Glass Heat treatment Near band edge emission Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Photoluminescence Physics Vanadium Zinc Zinc oxide ZnO-based scintilator |
Title | Preparation, heat treatment and photoluminescence properties of V-doped ZnO–SiO2–B2O3 glasses |
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