Controllable and chemo-selective conversion of sodium sulfinates to disulfides or thiosulfonates by a solvent-free mechanochemical approach

A solvent-free ball-milling method for synthesizing structurally diverse disulfide and thiosulfonate derivatives from readily available, odorless sodium sulfinates has been developed. This convenient mechanochemical protocol allows the rapid and chemo-selective construction of disulfides and thiosul...

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Bibliographic Details
Published inTetrahedron Vol. 139; pp. 133434 - 133441
Main Authors Wang, Jinjing, Liu, Xiongbo, Yang, Shikai, Yu, Ao, Li, Jinshan, Liu, Hongtao, Li, Jianwei, Jia, Chunman
Format Journal Article
LanguageEnglish
Published OXFORD Elsevier Ltd 12.06.2023
Elsevier
Subjects
Chemistry
Chemistry, Organic
Controllable synthesis
Disulfide
Mechanochemistry
Physical Sciences
Science & Technology
Solvent-free method
Thiosulfonate
Thiosulfonate
Mechanochemistry
Controllable synthesis
Disulfide
Solvent-free method
ONE-POT
UNSYMMETRICAL DISULFIDES
CATALYZED REGIOSELECTIVE SULFENYLATION
EFFICIENT
INDOLES
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Summary:A solvent-free ball-milling method for synthesizing structurally diverse disulfide and thiosulfonate derivatives from readily available, odorless sodium sulfinates has been developed. This convenient mechanochemical protocol allows the rapid and chemo-selective construction of disulfides and thiosulfonates. [Display omitted]
ISSN:0040-4020
1464-5416
DOI:10.1016/j.tet.2023.133434