Synthesis of TiN/N-doped TiO2 composite films as visible light active photocatalyst
Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO 2) composite films were synthesized for visible light photodegradation applications. Thin films of TiN were sputter-deposited on precleaned glass substrates in an admixture of argon and nitrogen gases. The grown TiN films were subsequen...
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| Published in | Journal of vacuum science and technology. B, Nanotechnology & microelectronics Vol. 38; no. 6 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.11.2020
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| Abstract | Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO
2) composite films were synthesized for visible light photodegradation applications. Thin films of TiN were sputter-deposited on precleaned glass substrates in an admixture of argon and nitrogen gases. The grown TiN films were subsequently oxidized in air at 350
°C at 15, 30, and 60 min. Raman spectral analysis revealed the formation of TiO
2 with anatase structure at 15 min and transitioned to the rutile structure at longer oxidation times. X-ray photoelectron spectral analysis revealed the formation of N-doped TiO
2 from the oxidized Ti. Visible light-induced photodegradation of methylene blue as test analyte showed 30% removal efficiency after exposure to visible light after 2.5 h. The highest degradation efficiency was observed when the anatase phase of TiO
2 is the dominant phase in the film. Moreover, N-doping realized the visible light sensitivity of TiO
2. This makes the composite film ideal for solar light-driven photodegradation of organic contaminants in wastewater. |
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| AbstractList | Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO
2) composite films were synthesized for visible light photodegradation applications. Thin films of TiN were sputter-deposited on precleaned glass substrates in an admixture of argon and nitrogen gases. The grown TiN films were subsequently oxidized in air at 350
°C at 15, 30, and 60 min. Raman spectral analysis revealed the formation of TiO
2 with anatase structure at 15 min and transitioned to the rutile structure at longer oxidation times. X-ray photoelectron spectral analysis revealed the formation of N-doped TiO
2 from the oxidized Ti. Visible light-induced photodegradation of methylene blue as test analyte showed 30% removal efficiency after exposure to visible light after 2.5 h. The highest degradation efficiency was observed when the anatase phase of TiO
2 is the dominant phase in the film. Moreover, N-doping realized the visible light sensitivity of TiO
2. This makes the composite film ideal for solar light-driven photodegradation of organic contaminants in wastewater. Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO2) composite films were synthesized for visible light photodegradation applications. Thin films of TiN were sputter-deposited on precleaned glass substrates in an admixture of argon and nitrogen gases. The grown TiN films were subsequently oxidized in air at 350 °C at 15, 30, and 60 min. Raman spectral analysis revealed the formation of TiO2 with anatase structure at 15 min and transitioned to the rutile structure at longer oxidation times. X-ray photoelectron spectral analysis revealed the formation of N-doped TiO2 from the oxidized Ti. Visible light-induced photodegradation of methylene blue as test analyte showed 30% removal efficiency after exposure to visible light after 2.5 h. The highest degradation efficiency was observed when the anatase phase of TiO2 is the dominant phase in the film. Moreover, N-doping realized the visible light sensitivity of TiO2. This makes the composite film ideal for solar light-driven photodegradation of organic contaminants in wastewater. |
| Author | Edañol, Yasmin D. Panghulan, Glenson R. Vasquez, Magdaleno R. Payawan, Leon M. Chanlek, Narong |
| Author_xml | – sequence: 1 givenname: Glenson R. surname: Panghulan fullname: Panghulan, Glenson R. email: grpanghulan@up.edu.ph organization: Department of Mining, Metallurgical, and Materials Engineering, College of Engineering, University of the Philippines, Diliman – sequence: 2 givenname: Magdaleno R. surname: Vasquez fullname: Vasquez, Magdaleno R. organization: Department of Mining, Metallurgical, and Materials Engineering, College of Engineering, University of the Philippines, Diliman – sequence: 3 givenname: Yasmin D. surname: Edañol fullname: Edañol, Yasmin D. organization: Natural Sciences Research Institute, College of Science, University of the Philippines, Diliman – sequence: 4 givenname: Narong surname: Chanlek fullname: Chanlek, Narong organization: Synchrotron Light Research Institute – sequence: 5 givenname: Leon M. surname: Payawan fullname: Payawan, Leon M. organization: Institute of Chemistry, College of Science, University of the Philippines, Diliman |
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| Snippet | Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO
2) composite films were synthesized for visible light photodegradation applications. Thin films... Titanium nitride/nitrogen-doped titanium oxide (TiN/N-doped TiO2) composite films were synthesized for visible light photodegradation applications. Thin films... |
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| Title | Synthesis of TiN/N-doped TiO2 composite films as visible light active photocatalyst |
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