Synthesis and Structure of Phosphito- and Thiophosphatocavitands

Phosphitocavitands, which on sulfurization result in all-cis-thiophosphatocavitands, have been obtained by phosphocyclization of octahydroxytetramethyl[14] metacyclophane with amides of phosphorous acid, as confirmed by 1H and 31P NMR spectroscopy and X-ray analysis.

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Published inMendeleev communications Vol. 5; no. 4; pp. 131 - 133
Main Authors Nifantyev, Eduard E., Maslennikova, Vera I., Panina, Elena V., Bekker, Anna R., Vasyanina, Larisa K., Lysenko, Konstantin A., Antipin, Mikhail Yu, Struchkov, Yurii T.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 1995
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Summary:Phosphitocavitands, which on sulfurization result in all-cis-thiophosphatocavitands, have been obtained by phosphocyclization of octahydroxytetramethyl[14] metacyclophane with amides of phosphorous acid, as confirmed by 1H and 31P NMR spectroscopy and X-ray analysis.
ISSN:0959-9436
DOI:10.1070/MC1995v005n04ABEH000490