Performance and Microstructure Variation with Maximum Heat Treatment Temperature for Recent Bi-2212 Round Wires

• Published in: IEEE transactions on applied superconductivity Vol. 33; no. 5; pp. 1 - 5
• Main Authors: Jiang, Jianyi, Hossain, S. Imam, Barua, Shaon, Oloye, T. Abiola, Kvitkovic, Jozef, Kametani, Fumitake, Trociewitz, Ulf P., Hellstrom, Eric E., Larbalestier, David C., Bugaris, Daniel E., Goggin, Claudia, Huang, Yibing, Parrell, Jeff A., Shen, Tengming
• Format: Journal Article
• Language: English
• Published: New York IEEE 01.08.2023; The Institute of Electrical and Electronics Engineers, Inc. (IEEE)
• Subjects: Bi-2212 wire; Billets; Bismuth strontium calcium copper oxide; Cables; Coils; Conductors; Cooling rate; critical current density; Filaments; Filling; Heat treating; Heat treatment; High temperature; Microstructure; Powders; superconducting magnet; Superconducting magnets; Superconductor; Wire; Wires
• ISSN: 1051-8223; 1558-2515
• DOI: 10.1109/TASC.2023.3236870

Bi-2212 is the only high temperature superconducting wire with the round geometry. It is multifilamentary, available in a wide range of fine filaments and twisted filament architectures and can be made into Rutherford and other cables. The properties of Bi-2212 conductors depend on powder quality, conductor fabrication and heat treatment. The heat treatment is still complex but much better understood, particularly the vital parameters of the maximum heat treatment temperature ( T max ), time-in-the-melt ( t melt ) and the cooling rate as Bi-2212 reforms on cooling. Here we report on the performance and microstructure variation with heat treatments for more than a dozen wires made with powders produced by Engi-Mat in recent years. Wire architectures include 37x18, 55x18 and 85x18 and wire diameters range from 0.8 to 1.0 mm. T max was varied between 884 and 897 °C. Wires with smaller filament diameter showed a peak J E at the low end of T ma x and also a J E that was more sensitive to T max . J E ( T max ) plots for all recent wires show a plateau between T max of 886 and 894 °C, where J E (4.2 K, 5 T) is 1100 - 1400 A/mm 2 . Some wires with filament size of 13 - 15 μm showed a 10 °C heat treatment window ( Δ T max ) with a plateau J E (4.2 K, 5 T) of about 1100 A/mm 2 .