Microstructure and Mechanical Properties of Powder Metallurgical TiAl-Based Alloy Made by Micron Bimodal-Sized Powders

• Published in: Journal of materials engineering and performance Vol. 30; no. 1; pp. 269 - 280
• Main Authors: Ren, Yibo, Han, Ying, Yan, Shun, Sun, Jiapeng, Duan, Zhenxin, Chen, Hua, Ran, Xu
• Format: Journal Article
• Language: English
• Published: New York Springer US 2021
• Subjects: Characterization and Evaluation of Materials; Chemistry and Materials Science; Corrosion and Coatings; Engineering Design; Materials Science; Quality Control; Reliability; Safety and Risk; Tribology; powder metallurgy; mechanical property; bimodal grain microstructure; TiAl alloy
• ISSN: 1059-9495; 1544-1024
• DOI: 10.1007/s11665-020-05342-3

Three powder metallurgical Ti-48Al-2Cr-2Nb compacts were prepared using spherical pre-alloyed powders, mechanically milled powders, and a mixture of the spherical pre-alloyed powders and the mechanical milled powders in a weight ratio of 1:4. Different microstructures corresponding to coarse grains, ultrafine grains, and bimodal-size grains, respectively, were obtained. The compact with a bimodal grain structure exhibits a good combination of high-yield compressive strength (~ 1393 MPa) and improved compression ratio to fracture (~ 13.9%) at room temperature due to the effects of back-stress and ductile γ -TiAl single-phase layer generated near the ultrafine/coarse grain interface. At high temperatures, the compressive properties of the compact with the bimodal grain size distribution are sensitive to the temperature. A relatively high deformation resistance is achieved at 750 °C. At this temperature, the coarse grain region of the bimodal grain-sized microstructure undergoes more strain, and the dynamic recrystallization is promoted with increasing strain, improving the ductility. By contrast, the ultrafine grains in the bimodal grain size microstructure dominate the dynamic softening when the temperature is higher than 850 °C due to their accelerated dynamic recrystallization and easy grain boundary slip that are responsible for the good formability and the sharp decrease in deformation resistance of this alloy.