Influence of activation of quartz grain surface on efficiency of the process of processing the quartz sand grains with fluoride technology

The influence of grinding the initial quartz sand on the degree of activation of the sand-grain surface during processing using a fluorinating reagent has been studied. Using the method of the synchronous thermal analysis, the technological parameters of producing ammonium hexafluorosilicate using m...

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Bibliographic Details
Published inTheoretical foundations of chemical engineering Vol. 47; no. 6; pp. 766 - 771
Main Authors Demyanova, L. P., Zaeva, A. S., Buinovskiy, A. S.
Format Journal Article
LanguageEnglish
Published Boston Springer US 01.11.2013
Subjects
Chemistry
Chemistry and Materials Science
Industrial Chemistry/Chemical Engineering
Fluorinating Agent
Differential Scanning Calorimetry Curve
Quartz Sand
Thermogravimetric Curf
Synchronous Thermal Analysis
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Summary:The influence of grinding the initial quartz sand on the degree of activation of the sand-grain surface during processing using a fluorinating reagent has been studied. Using the method of the synchronous thermal analysis, the technological parameters of producing ammonium hexafluorosilicate using mixtures of different fractions of sand at temperatures in the range of 25–400°C were examined. The investigation of intermediate phases, formed during the thermogravimetric experiment was carried out with the X-ray analysis. It was established that formation of ammonium hexafluorosilicate with crushed quartz sand occurs at temperatures of 30–40°C lower than the source conditions.
ISSN:0040-5795
1608-3431
DOI:10.1134/S0040579513040209