3,3′-bi(6,8-dialkyl-2,4-dioxa-7-thia-6,8-diazabicyclo[3.3.0]-octane-7,7-dioxides): Structure and synthesis

Derivatives of a new heterocyclic system, 3,3′-bi(6,8-dialkyl-2,4-dioxa-7-thia-6,8-diazabicyclo[3.3.0]-octane-7,7-dioxides), were synthesized by condensation of 1,3-dialkylsulfamides with glyoxal (as a dihydrate trimer). Their structure was investigated by spectral methods, XRD, and X-ray phase anal...

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Published inRussian journal of organic chemistry Vol. 45; no. 2; pp. 248 - 255
Main Authors Gazieva, G. A., Nelyubina, Yu. V., Kravchenko, A. N., Lysenko, K. A., Kolotyrkina, N. G., Belyakov, P. A., Korlyukov, A. A., Lebedev, O. V., Makhova, N. N.
Format Journal Article
LanguageEnglish
Published Dordrecht SP MAIK Nauka/Interperiodica 01.02.2009
Springer Nature
Subjects
Chemistry
Chemistry and Materials Science
Chemistry, Organic
Organic Chemistry
Physical Sciences
Science & Technology
Glyoxal
Thiram
Glycoluril
Eluent Ethyl Acetate
Heterocyclic System
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Summary:Derivatives of a new heterocyclic system, 3,3′-bi(6,8-dialkyl-2,4-dioxa-7-thia-6,8-diazabicyclo[3.3.0]-octane-7,7-dioxides), were synthesized by condensation of 1,3-dialkylsulfamides with glyoxal (as a dihydrate trimer). Their structure was investigated by spectral methods, XRD, and X-ray phase analysis of one among these compounds.
ISSN:1070-4280
1608-3393
DOI:10.1134/S107042800902016X