OXIDATION OF ALKYLCYANOHYDRAZINES TO AZO-BIS NITRILES USING OXONE®-POTASSIUM BROMIDE IN AQUEOUS MEDIUM

Azo-bis nitriles were prepared in good yields and high purity by oxidation of corresponding 1,2-bis-dialkylcyano hydrazines using oxone-potassium bromide in aqueous medium.

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Bibliographic Details
Published inSynthetic communications Vol. 32; no. 23; pp. 3643 - 3646
Main Authors Tamhankar, B. V., Desai, Uday V., Mane, R. B., Kulkarni, P. P., Wadgaonkar, P. P.
Format Journal Article
LanguageEnglish
Published PHILADELPHIA Taylor & Francis Group 01.01.2002
Taylor & Francis
Subjects
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
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Summary:Azo-bis nitriles were prepared in good yields and high purity by oxidation of corresponding 1,2-bis-dialkylcyano hydrazines using oxone-potassium bromide in aqueous medium.
ISSN:0039-7911
1532-2432
DOI:10.1081/SCC-120014980