Phenolic Compounds from Japanese Anise (Illicium anisatum L.) Leaves
Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform (CHCl3), ethylacetate (EtOAc) and H2O, and then freeze dried after concentration. A port...
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| Published in | Journal of the Korean Wood Science and Technology Vol. 47; no. 1; pp. 1 - 7 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English Korean |
| Published |
한국목재공학회
2019
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1017-0715 2233-7180 |
| DOI | 10.5658/WOOD.2019.47.1.1 |
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| Abstract | Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform (CHCl3), ethylacetate (EtOAc) and H2O, and then freeze dried after concentration. A portion of EtOAc (3.12 g) and H2O (6.08 g) soluble fractions were chromatographed on a Sephadex LH-20 column with various aqueous MeOH solution to isolate the compounds.
Compound 1 ((+)-catechin) was isolated from EtOAc soluble fraction. Compounds 2 (quercetin), 3 (quercitrin) and 4 (2''-O-rhamnosylvitexin) were isolated from H2O soluble fraction.
For the first time, quercitrin (3) and 2''-O-rhamnosylvitexin (4) of the isolated compounds were obtained from the extracts of japanese anise leaves. |
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| AbstractList | Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform ($CHCl_3$), ethylacetate (EtOAc) and $H_2O$, and then freeze dried after concentration. A portion of EtOAc (3.12 g) and $H_2O$ (6.08 g) soluble fractions were chromatographed on a Sephadex LH-20 column with various aqueous MeOH solution to isolate the compounds. Compound 1 ((+)-catechin) was isolated from EtOAc soluble fraction. Compounds 2 (quercetin), 3 (quercitrin) and 4 (2''-O-rhamnosylvitexin) were isolated from $H_2O$ soluble fraction. For the first time, quercitrin (3) and 2''-O-rhamnosylvitexin (4) of the isolated compounds were obtained from the extracts of japanese anise leaves. Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform (CHCl3), ethylacetate (EtOAc) and H2O, and then freeze dried after concentration. A portion of EtOAc (3.12 g) and H2O (6.08 g) soluble fractions were chromatographed on a Sephadex LH-20 column with various aqueous MeOH solution to isolate the compounds. Compound 1 ((+)-catechin) was isolated from EtOAc soluble fraction. Compounds 2 (quercetin), 3 (quercitrin) and 4 (2''-O-rhamnosylvitexin) were isolated from H2O soluble fraction. For the first time, quercitrin (3) and 2''-O-rhamnosylvitexin (4) of the isolated compounds were obtained from the extracts of japanese anise leaves. KCI Citation Count: 2 Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform (CHCl3), ethylacetate (EtOAc) and H2O, and then freeze dried after concentration. A portion of EtOAc (3.12 g) and H2O (6.08 g) soluble fractions were chromatographed on a Sephadex LH-20 column with various aqueous MeOH solution to isolate the compounds. Compound 1 ((+)-catechin) was isolated from EtOAc soluble fraction. Compounds 2 (quercetin), 3 (quercitrin) and 4 (2''-O-rhamnosylvitexin) were isolated from H2O soluble fraction. For the first time, quercitrin (3) and 2''-O-rhamnosylvitexin (4) of the isolated compounds were obtained from the extracts of japanese anise leaves. |
| Author | Seong-whan Shinn Young-Soo Bae Hee-Jeong Min |
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| Cites_doi | 10.1002/ptr.1592 10.1021/jf020850t 10.1016/S0040-4039(01)89037-7 10.2478/v10007-009-0022-y 10.1248/cpb.26.2671 10.1016/0040-4020(68)89022-2 10.1016/S0278-6915(03)00011-5 10.1007/BF02980043 10.5658/WOOD.2017.45.6.809 10.5658/WOOD.2017.45.1.96 10.1271/bbb.63.184 10.1016/S0367-326X(00)00224-0 10.5658/WOOD.2015.43.5.591 10.1016/j.foodchem.2008.09.077 10.1039/c39830000672 10.5658/WOOD.2015.43.4.494 10.5658/WOOD.2015.43.2.238 |
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| Title | Phenolic Compounds from Japanese Anise (Illicium anisatum L.) Leaves |
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