Fracture Load of Layered Glass-Ceramic Structures

• Published in: Strength of materials Vol. 54; no. 3; pp. 515 - 524
• Main Authors: Marocho, S. M. Salazar, Cesar, P. F., Griggs, J. A., Bottino, M. A.
• Format: Journal Article
• Language: English
• Published: New York Springer US 01.05.2022; Springer; Springer Nature B.V
• Subjects: Cements; Ceramic bonding; Ceramic materials; Ceramics; Characterization and Evaluation of Materials; Chemistry and Materials Science; Classical Mechanics; Deionization; Disks; Failure modes; Glass ceramics; Materials Science; Mechanical properties; Porcelain; Resins; Solid Mechanics; Viscosity; Weibull modulus; viscosity; resin cement; porcelain; fracture load; bonding
• ISSN: 0039-2316; 1573-9325
• DOI: 10.1007/s11223-022-00426-y

The mechanical behavior and failure mode of multilayered bonded and non-bonded glass-ceramic structures after long-term water-aging is relevant considering how widely used these ceramics are in many fields. This work is focused on ceramic structures used in dentistry. The objective here was to determine the fracture load of ceramic structures not bonded and bonded to a dentin analog material (G10) using low (L) and high-viscosity (UH) dual-cured resin cements (C). Porcelain ( P ) disks were tested whether bonded or not bonded to G10, as follows: a) P – control group, b) P HF – acid etched, c) P · C L – HF and coated with C L , d) P·C UH – HF and coated with C UH , e) P · C L ·G10 – HF and bonded to G10 using C L , and f) P · C UH ·G10 – HF and bonded to G10 using C UH . The groups bonded to G10 were stored in deionized water for 24 h, 1, 3, and 6 months. The fracture load was examined using Weibull statistics. The Weibull modulus ( m ) for group P was similar to that of P HF and significantly higher than for P · C L and P · C UH . P · C L showed higher m than P · C UH . As for the characteristic fracture loads ( F 0 ), P and P HF showed statistically similar values that were significantly higher than those obtained for P · C L and P · C UH . For P · C UH ·G10, there was no effect of storage time on both the F 0 and m. For P · C L ·G10, storage time only caused significant changes in F 0 . After aging, there was no change in the mechanical behavior of the porcelain structures bonded to G10 using C UH . There was a decrease in F 0 over time when C L was used. These results reveal that the viscosity of the resin cement plays an important role in the mechanical behavior of the bonded porcelain structures. Overall, ceramic structures bonded using a high-viscosity dual-cured resin cement seems to present better performance over time.