[2-(3,4-Dimethoxyphenyl)ethyl](3-{ N -[2-(3,4-dimethoxyphenyl)ethyl]carbamoyl}propyl)azanium chloride dihydrate
The asymmetric unit of the title hydrated salt, C 24 H 35 N 2 O 5 + ·Cl − ·2H 2 O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water molecules. In the crystal, one pair of lattice water molecules and two chloride anions form a f...
Saved in:
| Published in | Acta crystallographica. Section E, Structure reports online Vol. 70; no. 2; p. o232 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
International Union of Crystallography
01.02.2014
|
| Online Access | Get full text |
Cover
Loading…
| Summary: | The asymmetric unit of the title hydrated salt, C
24
H
35
N
2
O
5
+
·Cl
−
·2H
2
O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water molecules. In the crystal, one pair of lattice water molecules and two chloride anions form a four-membered centrosymmetric hydrogen-bond cycle. In addition, O—H...O, N—H...O and N—H...Cl hydrogen bonds involving the N—H groups, the water molecules and the C=O group are observed. As a result, a hydrogen-bonded layer parallel to (100) is formed. The thickness of such a layer corresponds to the length of the
a
axis [21.977 (3) Å]. |
|---|---|
| ISSN: | 1600-5368 1600-5368 |
| DOI: | 10.1107/S1600536814001998 |