Microwave-assisted solid-phase chemistry for rapid efficient generation and trapping of sulfenic acids

An easy two step procedure starting from commercially available REM resin allowed the preparation of suitable solid-supported precursors of sulfenic acids. Their microwave-assisted generation and trapping resulted superior to the conventional solution-phase procedure and thermal heating in terms of...

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Bibliographic Details
Published inJournal of sulfur chemistry Vol. 27; no. 5; pp. 393 - 400
Main Authors Menichetti, Stefano, Aversa, Maria Chiara, Bonaccorsi, Paola, Lamanna, Giuseppe, Moraru, Alina
Format Journal Article
LanguageEnglish
Published Taylor & Francis 01.10.2006
Subjects
Green chemistry
Microwaves
Solid-phase
Sulfenic acids
Sulfoxides
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Summary:An easy two step procedure starting from commercially available REM resin allowed the preparation of suitable solid-supported precursors of sulfenic acids. Their microwave-assisted generation and trapping resulted superior to the conventional solution-phase procedure and thermal heating in terms of simplicity, eco-compatibility, and final yields.
ISSN:1741-5993
1741-6000
DOI:10.1080/17415990600908714