Hydrolysis of polycarbonate in sub-critical water in fused silica capillary reactor with in situ Raman spectroscopy

The advantages of using fused silica capillary reactor (FSCR) instead of conventional autoclave for studying chemical reactions at elevated pressure and temperature conditions were demonstrated in this study, including the allowance for visual observation under a microscope and in situ Raman spectro...

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Published inGreen chemistry : an international journal and green chemistry resource : GC Vol. 11; no. 8; pp. 1105 - 1107
Main Authors Pan, Zhiyan, Chou, I-Ming, Burruss, Robert C.
Format Journal Article
LanguageEnglish
Published 01.01.2009
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Summary:The advantages of using fused silica capillary reactor (FSCR) instead of conventional autoclave for studying chemical reactions at elevated pressure and temperature conditions were demonstrated in this study, including the allowance for visual observation under a microscope and in situ Raman spectroscopic characterization of polycarbonate and coexisting phases during hydrolysis in subcritical water.
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ISSN:1463-9262
1463-9270
DOI:10.1039/b904810n