Ceria supported nickel catalysts for CO removal from H2-rich gas
CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia, the complexing method using urea, the complexing method using citric acid and the precipitation method using ammonium carbonate, were adopted...
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| Published in | Journal of rare earths Vol. 34; no. 12; pp. 1213 - 1220 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.12.2016
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| Abstract | CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia, the complexing method using urea, the complexing method using citric acid and the precipitation method using ammonium carbonate, were adopted to prepare samples NiO/CeO2 as catalyst precursors for removal of CO from H2-rich gas via selective methanation reaction. The sample NiO/CeO2 prepared by the precipitation method using aqueous ammonia as precipitant exhibited the highest catalytic activity both for CO methanation and for CO2 methanation after reduction prior to the catalytic reaction. Chlorine ion was then doped to suppress CO2 conversion. Effect of chlorine doping was investigated. Over the optimal catalyst 40%Ni（Cl（0.2））/CeO2, CO in the H2-rich gas was removed to below 10 ppm with selectivity of 60% or higher at reaction temperatures 230–250 ℃ in the test period of 75 h. |
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| AbstractList | CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia, the complexing method using urea, the complexing method using citric acid and the precipitation method using ammonium carbonate, were adopted to prepare samples NiO/CeO2 as catalyst precursors for removal of CO from H2-rich gas via selective methanation reaction. The sample NiO/CeO2 prepared by the precipitation method using aqueous ammonia as precipitant exhibited the highest catalytic activity both for CO methanation and for CO2 methanation after reduction prior to the catalytic reaction. Chlorine ion was then doped to suppress CO2 conversion. Effect of chlorine doping was investigated. Over the optimal catalyst 40%Ni（Cl（0.2））/CeO2, CO in the H2-rich gas was removed to below 10 ppm with selectivity of 60% or higher at reaction temperatures 230–250 ℃ in the test period of 75 h. CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia, the complexing method using urea, the complexing method using citric acid and the precipitation method using ammonium carbonate, were adopted to prepare samples NiO/CeO2 as catalyst precursors for removal of CO from H2-rich gas via selective methanation reaction. The sample NiO/CeO2 prepared by the precipitation method using aqueous ammonia as precipitant exhibited the highest catalytic activity both for CO methanation and for CO2 methanation after reduction prior to the catalytic reaction. Chlorine ion was then doped to suppress CO2 conversion. Effect of chlorine doping was investigated. Over the optimal catalyst 40%Ni(Cl0.2)/CeO2, CO in the H2-rich gas was removed to below 10 ppm with selectivity of 60% or higher at reaction temperatures 230–250 °C in the test period of 75 h. A deep removal of CO was achieved over catalysts Ni(Clx)/CeO2 due to the suppression effect of chlorine ions on adsorption of CO2 |
| Author | 高志明 代倩子 马宏伟 李展平 |
| AuthorAffiliation | School of Chemistry, Beijing hlstitute of Technology, Beijing 102488, China Analysis Center; Tsinghua University, Beijing 100084, China |
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| CitedBy_id | crossref_primary_10_1016_j_jre_2017_12_006 crossref_primary_10_1016_j_apcata_2017_02_001 crossref_primary_10_1021_acscatal_4c02449 crossref_primary_10_1016_j_apcata_2018_02_032 crossref_primary_10_1039_D3CY01103H crossref_primary_10_1016_j_apcatb_2017_09_052 crossref_primary_10_1002_ente_201700088 crossref_primary_10_1016_j_ijhydene_2018_12_192 crossref_primary_10_3390_hydrogen4020027 crossref_primary_10_1016_j_jre_2018_03_017 crossref_primary_10_1016_S1002_0721_17_61002_0 crossref_primary_10_1016_j_ijhydene_2018_03_185 crossref_primary_10_1016_j_catcom_2018_09_011 crossref_primary_10_1016_j_mcat_2024_114396 crossref_primary_10_1016_j_ijhydene_2022_08_271 crossref_primary_10_1002_slct_201904630 |
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| Keywords | nickel adsorption ceria chlorine doping CO selective methanation rare earths |
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| Notes | 11-2788/TF CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia, the complexing method using urea, the complexing method using citric acid and the precipitation method using ammonium carbonate, were adopted to prepare samples NiO/CeO2 as catalyst precursors for removal of CO from H2-rich gas via selective methanation reaction. The sample NiO/CeO2 prepared by the precipitation method using aqueous ammonia as precipitant exhibited the highest catalytic activity both for CO methanation and for CO2 methanation after reduction prior to the catalytic reaction. Chlorine ion was then doped to suppress CO2 conversion. Effect of chlorine doping was investigated. Over the optimal catalyst 40%Ni（Cl（0.2））/CeO2, CO in the H2-rich gas was removed to below 10 ppm with selectivity of 60% or higher at reaction temperatures 230–250 ℃ in the test period of 75 h. CO selective methanation; nickel; ceria; chlorine doping; adsorption; rare earths GAO Zhiming,DAI Qianzi,MA Hongwei,LI Zhanping （1. School of Chemistry; Beijing btstitute of Technology, Beijing 102488, China; 2. Analysis Center; Tsinghua University, Beijing 100084, China） |
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| Snippet | CO in H2-rich gas must be removed to meet various requirements in industrial applications. Four methods, i.e., the precipitation method using aqueous ammonia,... |
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| SubjectTerms | adsorption ceria chlorine doping CO selective methanation CO2 nickel rare earths 富氢气体 尿素络合法 氧化铈 氨水沉淀法 甲烷化反应 负载 镍催化剂 |
| Title | Ceria supported nickel catalysts for CO removal from H2-rich gas |
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