Synthesis and structural characterisation of platinum silasesquioxane complexes
The reaction of partially condensed silasesquioxanes of the type [(R7Si7O9)-Si-1(OH)(2)(OR2)] (R-1 = c-C5H9, C-C6H11; R-2 = H, SiMe3) with either [Pt(dppe)(CO3)] or [Pt(dppe)Cl-2]/Ag2O leads to the formation of [(R7Si7O9)-Si-1(OR2)O2Pt(dppe)], crystallographically characterised for R-1 = c-C5H9; R-2...
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| Published in | Chemical communications (Cambridge, England) no. 23; pp. 2627 - 2628 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Royal Soc Chemistry
07.12.1998
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| Abstract | The reaction of partially condensed silasesquioxanes of the type [(R7Si7O9)-Si-1(OH)(2)(OR2)] (R-1 = c-C5H9, C-C6H11; R-2 = H, SiMe3) with either [Pt(dppe)(CO3)] or [Pt(dppe)Cl-2]/Ag2O leads to the formation of [(R7Si7O9)-Si-1(OR2)O2Pt(dppe)], crystallographically characterised for R-1 = c-C5H9; R-2 = SiMe3, providing unprecedented routes to late transition metal silasesquioxane complexes. |
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| AbstractList | The reaction of partially condensed silasesquioxanes of the type [(R7Si7O9)-Si-1(OH)(2)(OR2)] (R-1 = c-C5H9, C-C6H11; R-2 = H, SiMe3) with either [Pt(dppe)(CO3)] or [Pt(dppe)Cl-2]/Ag2O leads to the formation of [(R7Si7O9)-Si-1(OR2)O2Pt(dppe)], crystallographically characterised for R-1 = c-C5H9; R-2 = SiMe3, providing unprecedented routes to late transition metal silasesquioxane complexes. |
| Author | Lutz, M van Santen, RA Palmer, MT Kooijman, H Burrows, AD Abbenhuis, HCL Spek, AL |
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| References | KEMMITT, RDW (WOS:A1992HP10000010) 1992 FEHER, FJ (WOS:A1991FW22000070) 1991; 10 FEHER, FJ (WOS:A1989T533900028) 1989; 111 BRYNDZA, HE (WOS:A1986D522600018) 1986; 108 ANDREWS, MA (WOS:A1991EY68100009) 1991; 10 Burrows, AD (WOS:A1996TQ67500025) 1996 Burrows, AD (WOS:A1997WW48300007) 1997 FEHER, FJ (WOS:A1995RW66200006) 1995; 14 ANDREWS, MA (WOS:A1994NV42100025) 1994; 116 FEHER, FJ (WOS:A1986C923200062) 1986; 108 |
| References_xml | – volume: 10 start-page: 2526 year: 1991 ident: WOS:A1991FW22000070 article-title: FACILE SYNTHESES OF NEW INCOMPLETELY CONDENSED POLYHEDRAL OLIGOSILSESQUIOXANES - [(CCYCLO-C5H9)7SI7O9(OH)3], [(CYCLO-C7H13)7SI7O9(OH)3], AND [(CYCLO-C7H13)6SI6O7(OH)4] publication-title: ORGANOMETALLICS contributor: fullname: FEHER, FJ – start-page: 149 year: 1996 ident: WOS:A1996TQ67500025 article-title: Molecular recognition of 2,6-diaminopyridine by platinum orotate complexes publication-title: JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS contributor: fullname: Burrows, AD – volume: 14 start-page: 3239 year: 1995 ident: WOS:A1995RW66200006 article-title: SILASESQUIOXANES AS LIGANDS IN INORGANIC AND ORGANOMETALLIC CHEMISTRY publication-title: POLYHEDRON contributor: fullname: FEHER, FJ – volume: 10 start-page: 387 year: 1991 ident: WOS:A1991EY68100009 article-title: PHOTOINDUCED NET [2 + 2 + 2] CYCLOREVERSION OF PLATINUM(II) GLYCOLATE COMPLEXES - A NEW APPROACH TO THE GENERATION OF REDUCED, COORDINATIVELY UNSATURATED METAL SPECIES AND THE ACTIVATION OF CARBOHYDRATE CARBON-CARBON SINGLE BONDS publication-title: ORGANOMETALLICS contributor: fullname: ANDREWS, MA – volume: 108 start-page: 3850 year: 1986 ident: WOS:A1986C923200062 article-title: POLYHEDRAL OLIGOMETALLASILSESQUIOXANES (POMSS) AS MODELS FOR SILICA-SUPPORTED TRANSITION-METAL CATALYSTS - SYNTHESIS AND CHARACTERIZATION OF (C5ME5)ZR[(SI7O12)(C-C6H11)7] publication-title: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY contributor: fullname: FEHER, FJ – start-page: 1295 year: 1997 ident: WOS:A1997WW48300007 article-title: Platinum(II) phosphine complexes of dicarboxylates and ammonia: Crystal structures of [{Pt(PPh3)(2)}(2){mu-1,3-(O2C)(2)C6H4}(2)], [{Pt(PPh3)(2)-(NH3)}(2){mu-1,4-(O2C)(2)C6H4}][PF6](2) and cis-[Pt(PPh3)(2)(NH3)(2)][NO3](2) publication-title: JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS contributor: fullname: Burrows, AD – volume: 111 start-page: 1741 year: 1989 ident: WOS:A1989T533900028 article-title: SILSESQUIOXANES AS MODELS FOR SILICA SURFACES publication-title: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY contributor: fullname: FEHER, FJ – volume: 116 start-page: 5730 year: 1994 ident: WOS:A1994NV42100025 article-title: REGIOSELECTIVE COMPLEXATION OF UNPROTECTED CARBOHYDRATES BY PLATINUM(II) - SYNTHESIS, STRUCTURE, COMPLEXATION EQUILIBRIA, AND HYDROGEN-BONDING IN CARBONATE-DERIVED BIS(PHOSPHINE)PLATINUM(II) DIOLATE AND ALDITOLATE COMPLEXES publication-title: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY contributor: fullname: ANDREWS, MA – volume: 108 start-page: 4805 year: 1986 ident: WOS:A1986D522600018 article-title: BETA-HYDRIDE ELIMINATION FROM METHOXO VS ETHYL LIGANDS - THERMOLYSIS OF (DPPE)PT(OCH3)2, (DPPE)PT(CH2CH3)(OCH3) AND (DPPE)PT(CH2CH3)2 publication-title: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY contributor: fullname: BRYNDZA, HE – start-page: 1165 year: 1992 ident: WOS:A1992HP10000010 article-title: SYNTHESIS AND REACTIVITY OF N-ACETYLAMINO ACIDATE(2-) AND RELATED COMPLEXES OF PLATINUM(II) publication-title: JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS contributor: fullname: KEMMITT, RDW |
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