Crystal and molecular structure of benzoaza-12-crown-4 hydrochloride

The X-ray crystallographic analysis of benzoaza-12-crown-4 hydrochloride crystals is performed for the first time: space group P 1, a = 7.7497(4) Å, b = 9.2224(5) Å, c = 10.2395(5) Å, α = 99.3965(10)°, β = 101.8387(11)°, γ = 112.6470(10)°, V = 636,81(6) Å 3 , Z = 2, ρ calc = 1.355 g/cm 3 . The confo...

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Bibliographic Details
Published inJournal of structural chemistry Vol. 56; no. 1; pp. 142 - 147
Main Authors Glushko, V. N., Sadovskaya, N. Yu, Blokhina, L. I., Anan‘ev, I. V.
Format Journal Article
LanguageEnglish
Published Moscow Pleiades Publishing 2015
Subjects
Atomic
Atomic/Molecular Structure and Spectra
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Molecular
Optical and Plasma Physics
Physical Chemistry
Solid State Physics
X-ray crystallographic analysis
benzoaza-12-crown-4
crown ethers
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Summary:The X-ray crystallographic analysis of benzoaza-12-crown-4 hydrochloride crystals is performed for the first time: space group P 1, a = 7.7497(4) Å, b = 9.2224(5) Å, c = 10.2395(5) Å, α = 99.3965(10)°, β = 101.8387(11)°, γ = 112.6470(10)°, V = 636,81(6) Å 3 , Z = 2, ρ calc = 1.355 g/cm 3 . The conformation of the 12-membered ring of the molecule is determined.
ISSN:0022-4766
1573-8779
DOI:10.1134/S0022476615010205