Tensile, flexural and fracture properties of MEX-printed PLA-based composites

• Published in: Theoretical and applied fracture mechanics Vol. 132; p. 104478
• Main Authors: Stoia, Dan Ioan, Linul, Emanoil
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.08.2024
• Subjects: Failure mechanisms; Fracture properties; Macrostructural analysis; Material extrusion; PLA composites; MEX; MEX-AM; PLA composites; PLA; TPB; BP; GF-PLA; NR-PLA; FPZ; ABS; Tg; DSC; Tm; BP-PLA; ID; Failure mechanisms; CB; CF-PLA; GF; SENB; CF; AM; GnP-PLA; TGA; Material extrusion; PA; 3D; LD; MWCNT; LG; Macrostructural analysis; Fracture properties; DB
• ISSN: 0167-8442; 1872-7638
• DOI: 10.1016/j.tafmec.2024.104478

•Fracture properties of MEX-printed PLA-based composites were experimentally investigated.•Layer growth and material type significantly influence the mechanical behavior of the samples.•PLA material gives the best strength properties, while CF-PLA stands out as the stiffest material.•Distinct failure mechanisms associated with each test type, material and layer growth were identified. Due to the continuous development of material extrusion-additive manufacturing (MEX-AM) technology, the fracture behavior of polymeric parts, and especially of their associated composites, presents some shortcomings and also a challenge in the field. In this paper, the fracture properties of non-reinforced (NR) and reinforced Polylactic Acid (PLA) samples manufactured by MEX-AM process are investigated through tensile, flexural and fracture mechanics tests. The samples are reinforced with glass fibers (GF-PLA), carbon fibers (CF-PLA) and bronze particles (BP-PLA), and tested parallel (named FLAT for all tests) and normal (named UPRIGHT for tensile test, and ON-EDGE for flexural and fracture mechanics tests) to the layer growth (LG). It was found that regardless of the type of test, the LG and the material significantly influence the mechanical properties and collapse modes of the MEX-printed samples. It was obtained that the parallel-LG load is favorable for the tensile and flexural tests, and the normal-LG for the fracture mechanics tests. Overall, the NR-PLA material gives the best strength, strain and energy absorption properties, CF-PLA stands out as the stiffest material, while BP-PLA presents the minimum performances for almost all properties. The macroscopic analyzes of the fractured samples clearly highlight distinct failure mechanisms associated with each type of test, material and LG. From the analysis of the mechanical behavior and macrostructural images, CF-PLA was identified as the most brittle material, and NR-PLA the most ductile.