Copper(II) alkyl- and benzylnitrosohy-droxylaminates as precursors for the synthesis of copper(i) oxide micro- and nanoparticles of various morphologies

We describe the thermal decomposition of a number of copper(II) alkyl- and benzylnitrosohy-droxylaminates via thermostating in polyethylene glycol and 2-dodecyl-1H-imidazole for various lengths of time. This process is shown to lead to the formation of copper(I) oxide nanoparticles, which have been...

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Bibliographic Details
Published inInorganic materials Vol. 50; no. 11; pp. 1093 - 1098
Main Authors Kovalchukova, O. V., Bostanabad, Ali Sheikh, Lobanov, N. N., Rudakova, T. A., Strashnov, P. V., Skarzhevskii, Yu. A., Zyuzin, I. N.
Format Journal Article
LanguageEnglish
Published Moscow Pleiades Publishing 01.11.2014
Subjects
Chemistry
Chemistry and Materials Science
Industrial Chemistry/Chemical Engineering
Inorganic Chemistry
Materials Science
Chemical Loop Combustion
Oxide Nanoparticles
Metal Oxide Nanoparticles
Copper Nanoparticles
Cuprous Oxide
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Summary:We describe the thermal decomposition of a number of copper(II) alkyl- and benzylnitrosohy-droxylaminates via thermostating in polyethylene glycol and 2-dodecyl-1H-imidazole for various lengths of time. This process is shown to lead to the formation of copper(I) oxide nanoparticles, which have been characterized by X-ray diffraction and electron spectroscopy. The starting copper(II) nitrosohydroxylaminates have been characterized by thermogravimetry.
ISSN:0020-1685
1608-3172
DOI:10.1134/S0020168514110090