Synthesis and Crystal Structure Hindered Amine with Methaerylate

The high pure hindered amine with methaerylate (2,2,6,6-tetramethylpiperidin-4-yl methacrylate) 4 was synthesized by a condensation reaction of 2,2,6,6-tetramethylpiperidin-4-ol and methacrylic anhydride via isolation of the salt (1:1) of 4 and methacrylic acid in an improved yield (total 80%). The...

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Published inAdvanced Materials Research Vol. 1095; pp. 381 - 384
Main Authors Lu, Guo Yuan, Chen, Qiang, Zhang, Xiu Qin, Jin, Ji, Xue, Wei Wei
Format Journal Article
LanguageEnglish
Published Zurich Trans Tech Publications Ltd 20.03.2015
Subjects
Amines
Anhydrides
Condensation
Crystal structure
Crystallography
Methacrylic acid
Synthesis
X-rays
Crystal Structure
Light Stabilizer
Hindered Amine
Methaerylate
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Summary:The high pure hindered amine with methaerylate (2,2,6,6-tetramethylpiperidin-4-yl methacrylate) 4 was synthesized by a condensation reaction of 2,2,6,6-tetramethylpiperidin-4-ol and methacrylic anhydride via isolation of the salt (1:1) of 4 and methacrylic acid in an improved yield (total 80%). The structure of the salt 4 of hindered amine was demonstrated by X-ray crystallographic analysis.
Bibliography:Selected, peer reviewed papers from the 2014 5th International Conference on Advances in Materials and Manufacturing (ICAMMP 2014), December 20-21, 2014, Fuzhou, China
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ISBN:3038354317
9783038354314
ISSN:1022-6680
1662-8985
1662-8985
DOI:10.4028/www.scientific.net/AMR.1095.381