Cyano-bridged polynuclear coordination compounds derived from paramagnetic [Mn(H 2 daptsc)] 2+ and photochromic [Fe(CN) 5 NO] 2− building blocks

Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H 2 daptsc) were used for the first time ever as building blocks to create polynuclear multifunctional molecular materials. Reactions of the paramagnetic [Mn( ii )(H 2 daptsc)(H 2 O) 2 ](ClO 4 )...

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Published inCrystEngComm Vol. 23; no. 14; pp. 2733 - 2745
Main Authors Sasnovskaya, Valentina D., Zorina, Leokadiya V., Simonov, Sergey V., Talantsev, Artem D., Mikhailov, Artem A., Kostin, Gennadiy A., Yagubskii, Eduard B.
Format Journal Article
LanguageEnglish
Published Cambridge Royal Society of Chemistry 01.01.2021
Subjects
Coordination compounds
Crystal structure
Crystallography
Magnetic properties
Manganese
Photochromism
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Abstract Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H 2 daptsc) were used for the first time ever as building blocks to create polynuclear multifunctional molecular materials. Reactions of the paramagnetic [Mn( ii )(H 2 daptsc)(H 2 O) 2 ](ClO 4 ) 2 and [Mn( ii )(H 2 daptsc)Cl 2 ] complexes with photochromic sodium nitroprusside Na 2 [Fe( ii )(CN) 5 NO] . 2H 2 O were studied. As a result, six polynuclear phases were obtained: {Mn(H 2 daptsc)Fe(CN) 5 NO} n ·0.5 n (MeOH)·0.5 n (H 2 O) ( 1 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} 3n ·8 n (MeOH) ( 2 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} 2n · n (MeOH)· n (H 2 O) ( 3 ), [Mn(H 2 daptsc)Cl] 2 [Fe(CN) 5 NO] ( 4 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} n ·2 n (H 2 O) ( 5 ) and {Mn(H 2 daptsc)Fe(CN) 5 NO} n · n (EtOH) ( 6 ). The crystal structures of the phases as well as the magnetic and photochromic properties of 1 and 4 were studied.
AbstractList Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H 2 daptsc) were used for the first time ever as building blocks to create polynuclear multifunctional molecular materials. Reactions of the paramagnetic [Mn( ii )(H 2 daptsc)(H 2 O) 2 ](ClO 4 ) 2 and [Mn( ii )(H 2 daptsc)Cl 2 ] complexes with photochromic sodium nitroprusside Na 2 [Fe( ii )(CN) 5 NO] . 2H 2 O were studied. As a result, six polynuclear phases were obtained: {Mn(H 2 daptsc)Fe(CN) 5 NO} n ·0.5 n (MeOH)·0.5 n (H 2 O) ( 1 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} 3n ·8 n (MeOH) ( 2 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} 2n · n (MeOH)· n (H 2 O) ( 3 ), [Mn(H 2 daptsc)Cl] 2 [Fe(CN) 5 NO] ( 4 ), {Mn(H 2 daptsc)Fe(CN) 5 NO} n ·2 n (H 2 O) ( 5 ) and {Mn(H 2 daptsc)Fe(CN) 5 NO} n · n (EtOH) ( 6 ). The crystal structures of the phases as well as the magnetic and photochromic properties of 1 and 4 were studied.
Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H2daptsc) were used for the first time ever as building blocks to create polynuclear multifunctional molecular materials. Reactions of the paramagnetic [Mn(ii)(H2daptsc)(H2O)2](ClO4)2 and [Mn(ii)(H2daptsc)Cl2] complexes with photochromic sodium nitroprusside Na2[Fe(ii)(CN)5NO].2H2O were studied. As a result, six polynuclear phases were obtained: {Mn(H2daptsc)Fe(CN)5NO}n·0.5n(MeOH)·0.5n(H2O) (1), {Mn(H2daptsc)Fe(CN)5NO}3n·8n(MeOH) (2), {Mn(H2daptsc)Fe(CN)5NO}2n·n(MeOH)·n(H2O) (3), [Mn(H2daptsc)Cl]2[Fe(CN)5NO] (4), {Mn(H2daptsc)Fe(CN)5NO}n·2n(H2O) (5) and {Mn(H2daptsc)Fe(CN)5NO}n·n(EtOH) (6). The crystal structures of the phases as well as the magnetic and photochromic properties of 1 and 4 were studied.
Author Yagubskii, Eduard B.
Zorina, Leokadiya V.
Simonov, Sergey V.
Mikhailov, Artem A.
Sasnovskaya, Valentina D.
Kostin, Gennadiy A.
Talantsev, Artem D.
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Snippet Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H 2 daptsc) were used for the first time ever as...
Heptacoordinated metal complexes with a pentadentate ligand 2,6-diacetylpyridine-bis(thiosemicarbazone) (H2daptsc) were used for the first time ever as...
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SubjectTerms Coordination compounds
Crystal structure
Crystallography
Magnetic properties
Manganese
Photochromism
Title Cyano-bridged polynuclear coordination compounds derived from paramagnetic [Mn(H 2 daptsc)] 2+ and photochromic [Fe(CN) 5 NO] 2− building blocks
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