Intramolekular stickstoffstabilisierte Organoaluminiumverbindungen mit Naphthyl‐, Benzyl‐ und Phenylliganden
N, N‐Dimethylnaphthylamin (1) reagiert mit Butyllithium zu Li(Et2O)C10H6NMe2‐8 (2). Die Umsetzung von 2 mit Et2AlCl und EtAlCl2 führt zu Et2AlC10H6NMe2‐8 (3) bzw. EtAl(C10H6NMe2‐8)2 (5) und mit iBu2AlCl wird iBu2AlC10H6NMe2‐8 (4) gebildet. 1 reagiert mit Me3Al zum entsprechenden Addukt Me3Al←N(C10H7...
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| Published in | Zeitschrift für anorganische und allgemeine Chemie (1950) Vol. 630; no. 8‐9; pp. 1196 - 1204 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
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Weinheim
WILEY‐VCH Verlag
01.08.2004
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| Abstract | N, N‐Dimethylnaphthylamin (1) reagiert mit Butyllithium zu Li(Et2O)C10H6NMe2‐8 (2). Die Umsetzung von 2 mit Et2AlCl und EtAlCl2 führt zu Et2AlC10H6NMe2‐8 (3) bzw. EtAl(C10H6NMe2‐8)2 (5) und mit iBu2AlCl wird iBu2AlC10H6NMe2‐8 (4) gebildet. 1 reagiert mit Me3Al zum entsprechenden Addukt Me3Al←N(C10H7)Me2 (6). LiCH2C6H4NMe2‐2 (7) und LiC6H4CH2NR2‐2 (R = Me (10), Et (12)) reagieren mit Me2AlCl, Et2AlCl und iBu2AlCl unter Bildung von R2AlCH2C6H4NMe2‐2 (R = Me (8), Et (9)), iBu2AlC6H4CH2NMe2‐2 (11) und Et2AlC6H4CH2NEt2‐2 (13). Die neuen Verbindungen wurden durch Elementaranalysen, 1H‐, 13C‐ und 27Al‐NMR‐Untersuchungen sowie massenspektrometrisch, 3 (zwei Modifikationen), 5 und 6 darüberhinaus durch Einkristall‐Röntgenstrukturanalyse charakterisiert.
Intramolecularly Nitrogen‐stabilized Organoaluminum Compounds containing Naphthyl, Benzyl, and Phenyl Ligands
N, N‐Dimethylnaphthylamin (1) reacts with Butyllithium to give Li(Et2O)C10H6NMe2‐8 (2). The reaction of 2 with Et2AlCl and EtAlCl2 yields Et2AlC10H6NMe2‐8 (3) and EtAl(C10H6NMe2‐8)2 (5), respectively; reaction with iBu2AlCl yields iBu2AlC10H6NMe2‐8 (4). 1 reacts with Me3Al to give the corresponding adduct Me3Al←N(C10H7)Me2 (6). LiCH2C6H4NMe2‐2 (7), LiC6H4CH2NR2‐2 (R = Me (10), Et (12)) react with Me2AlCl, Et2AlCl and iBu2AlCl under formation of R2AlCH2C6H4NMe2‐2 (R = Me (8), Et (9)), iBu2AlC6H4CH2NMe2‐2 (11) and Et2AlC6H4CH2NEt2‐2 (13), respectively. The new compounds were characterized by elemental analyses, 1H‐, 13C‐, and 27Al‐NMR spectroscopy, and mass spectrometry, the structures of 3 (two modifications), 5, and 6 were determined by single crystal X‐ray diffraction. |
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| AbstractList | N, N‐Dimethylnaphthylamin (1) reagiert mit Butyllithium zu Li(Et2O)C10H6NMe2‐8 (2). Die Umsetzung von 2 mit Et2AlCl und EtAlCl2 führt zu Et2AlC10H6NMe2‐8 (3) bzw. EtAl(C10H6NMe2‐8)2 (5) und mit iBu2AlCl wird iBu2AlC10H6NMe2‐8 (4) gebildet. 1 reagiert mit Me3Al zum entsprechenden Addukt Me3Al←N(C10H7)Me2 (6). LiCH2C6H4NMe2‐2 (7) und LiC6H4CH2NR2‐2 (R = Me (10), Et (12)) reagieren mit Me2AlCl, Et2AlCl und iBu2AlCl unter Bildung von R2AlCH2C6H4NMe2‐2 (R = Me (8), Et (9)), iBu2AlC6H4CH2NMe2‐2 (11) und Et2AlC6H4CH2NEt2‐2 (13). Die neuen Verbindungen wurden durch Elementaranalysen, 1H‐, 13C‐ und 27Al‐NMR‐Untersuchungen sowie massenspektrometrisch, 3 (zwei Modifikationen), 5 und 6 darüberhinaus durch Einkristall‐Röntgenstrukturanalyse charakterisiert.
Intramolecularly Nitrogen‐stabilized Organoaluminum Compounds containing Naphthyl, Benzyl, and Phenyl Ligands
N, N‐Dimethylnaphthylamin (1) reacts with Butyllithium to give Li(Et2O)C10H6NMe2‐8 (2). The reaction of 2 with Et2AlCl and EtAlCl2 yields Et2AlC10H6NMe2‐8 (3) and EtAl(C10H6NMe2‐8)2 (5), respectively; reaction with iBu2AlCl yields iBu2AlC10H6NMe2‐8 (4). 1 reacts with Me3Al to give the corresponding adduct Me3Al←N(C10H7)Me2 (6). LiCH2C6H4NMe2‐2 (7), LiC6H4CH2NR2‐2 (R = Me (10), Et (12)) react with Me2AlCl, Et2AlCl and iBu2AlCl under formation of R2AlCH2C6H4NMe2‐2 (R = Me (8), Et (9)), iBu2AlC6H4CH2NMe2‐2 (11) and Et2AlC6H4CH2NEt2‐2 (13), respectively. The new compounds were characterized by elemental analyses, 1H‐, 13C‐, and 27Al‐NMR spectroscopy, and mass spectrometry, the structures of 3 (two modifications), 5, and 6 were determined by single crystal X‐ray diffraction. Abstract N, N ‐Dimethylnaphthylamin ( 1 ) reagiert mit Butyllithium zu Li(Et 2 O)C 10 H 6 NMe 2 ‐8 ( 2 ). Die Umsetzung von 2 mit Et 2 AlCl und EtAlCl 2 führt zu Et 2 AlC 10 H 6 NMe 2 ‐8 ( 3 ) bzw. EtAl(C 10 H 6 NMe 2 ‐8) 2 ( 5 ) und mit i Bu 2 AlCl wird i Bu 2 AlC 10 H 6 NMe 2 ‐8 ( 4 ) gebildet. 1 reagiert mit Me 3 Al zum entsprechenden Addukt Me 3 Al←N(C 10 H 7 )Me 2 ( 6 ). LiCH 2 C 6 H 4 NMe 2 ‐2 ( 7 ) und LiC 6 H 4 CH 2 NR 2 ‐2 (R = Me ( 10 ), Et ( 12 )) reagieren mit Me 2 AlCl, Et 2 AlCl und i Bu 2 AlCl unter Bildung von R 2 AlCH 2 C 6 H 4 NMe 2 ‐2 (R = Me ( 8 ), Et ( 9 )), i Bu 2 AlC 6 H 4 CH 2 NMe 2 ‐2 ( 11 ) und Et 2 AlC 6 H 4 CH 2 NEt 2 ‐2 ( 13 ). Die neuen Verbindungen wurden durch Elementaranalysen, 1 H‐, 13 C‐ und 27 Al‐NMR‐Untersuchungen sowie massenspektrometrisch, 3 (zwei Modifikationen), 5 und 6 darüberhinaus durch Einkristall‐Röntgenstrukturanalyse charakterisiert. Intramolecularly Nitrogen‐stabilized Organoaluminum Compounds containing Naphthyl, Benzyl, and Phenyl Ligands N, N ‐Dimethylnaphthylamin ( 1 ) reacts with Butyllithium to give Li(Et 2 O)C 10 H 6 NMe 2 ‐8 ( 2 ). The reaction of 2 with Et 2 AlCl and EtAlCl 2 yields Et 2 AlC 10 H 6 NMe 2 ‐8 ( 3 ) and EtAl(C 10 H 6 NMe 2 ‐8) 2 ( 5 ), respectively; reaction with i Bu 2 AlCl yields i Bu 2 AlC 10 H 6 NMe 2 ‐8 ( 4 ). 1 reacts with Me 3 Al to give the corresponding adduct Me 3 Al←N(C 10 H 7 )Me 2 ( 6 ). LiCH 2 C 6 H 4 NMe 2 ‐2 ( 7 ), LiC 6 H 4 CH 2 NR 2 ‐2 (R = Me ( 10 ), Et ( 12 )) react with Me 2 AlCl, Et 2 AlCl and i Bu 2 AlCl under formation of R 2 AlCH 2 C 6 H 4 NMe 2 ‐2 (R = Me ( 8 ), Et ( 9 )), i Bu 2 AlC 6 H 4 CH 2 NMe 2 ‐2 ( 11 ) and Et 2 AlC 6 H 4 CH 2 NEt 2 ‐2 ( 13 ), respectively. The new compounds were characterized by elemental analyses, 1 H‐, 13 C‐, and 27 Al‐NMR spectroscopy, and mass spectrometry, the structures of 3 (two modifications), 5 , and 6 were determined by single crystal X‐ray diffraction. |
| Author | Schutte, Stefan Wassermann, Birgit C. Eichhorn, Jens Lange, Katharina C. H. Schumann, Herbert Köhler, Katrin Hummert, Markus Dechert, Sebastian |
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| Notes | Professor Reinhard Schmutzler zum 70. Geburtstag gewidmet |
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| Snippet | N, N‐Dimethylnaphthylamin (1) reagiert mit Butyllithium zu Li(Et2O)C10H6NMe2‐8 (2). Die Umsetzung von 2 mit Et2AlCl und EtAlCl2 führt zu Et2AlC10H6NMe2‐8 (3)... Abstract N, N ‐Dimethylnaphthylamin ( 1 ) reagiert mit Butyllithium zu Li(Et 2 O)C 10 H 6 NMe 2 ‐8 ( 2 ). Die Umsetzung von 2 mit Et 2 AlCl und EtAlCl 2 führt... |
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| SubjectTerms | Aluminum Crystal structures Intramolecular nitrogen stabilization NMR (multinuclear) |
| Title | Intramolekular stickstoffstabilisierte Organoaluminiumverbindungen mit Naphthyl‐, Benzyl‐ und Phenylliganden |
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