ChemInform Abstract: Optimization of a Pd-Catalyzed Intramolecular α-Arylation Synthesis of Tricyclo-[7.3.1.02.7]-trideca-2,4,6-trien-13-ones

Optimized and scalable reaction conditions are developed for the Pd‐catalyzed cyclization of 2‐(2‐halobenzyl)cyclohexanones and related heterocyclic substrates to tricyclic ketones (II) and (IV).

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Bibliographic Details
Published inChemInform Vol. 41; no. 45; p. no
Main Authors Powell, Noel A., Hagen, Timothy J., Ciske, Fred L., Cai, Cuiman, Duran, Joseph E., Holsworth, Daniel D., Leonard, Daniele, Kennedy, Robert M., Edmunds, Jeremy J.
Format Journal Article
LanguageEnglish
Published Weinheim WILEY-VCH Verlag 09.11.2010
WILEY‐VCH Verlag
Subjects
cycloalkylphenyl derivatives
fused pyridine derivatives
multi-membered O
multi‐membered O,S‐heterocycles (O or S ring members)
S-heterocycles (O or S ring members)
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Summary:Optimized and scalable reaction conditions are developed for the Pd‐catalyzed cyclization of 2‐(2‐halobenzyl)cyclohexanones and related heterocyclic substrates to tricyclic ketones (II) and (IV).
Bibliography:ark:/67375/WNG-43NKCVQS-K
istex:E82E0EC090E11D08775F11685363EA1515248DC7
ArticleID:CHIN201045083
ISSN:0931-7597
1522-2667
DOI:10.1002/chin.201045083