Synthesis of an AlN Polycrystalline Bulk Layer and Nanotubes by Using NH 3 and Bi
A bulk layer of aluminum nitride (AlN) polycrystals was synthesized on a boron nitride crucible surface by heating Al chunks with 5 mol% of bismuth at 1273 K for 3 h under NH 3 gas flow. The fragments of the layer were characterized by X‐ray diffraction, scanning electron microscopy, and transmissio...
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| Published in | Journal of the American Ceramic Society Vol. 92; no. 11; pp. 2578 - 2582 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.11.2009
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| Online Access | Get full text |
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| Abstract | A bulk layer of aluminum nitride (AlN) polycrystals was synthesized on a boron nitride crucible surface by heating Al chunks with 5 mol% of bismuth at 1273 K for 3 h under NH
3
gas flow. The fragments of the layer were characterized by X‐ray diffraction, scanning electron microscopy, and transmission electron microscopy. The platelet grains of AlN with a size of 0.1–1.0 μm and having preferred orientation of the
c
‐axis perpendicular to the layer were formed at the crucible side. Nanotubes 6–15 μm long and about 20–100 nm thick grew on the gas phase side of the layer. |
|---|---|
| AbstractList | A bulk layer of aluminum nitride (AlN) polycrystals was synthesized on a boron nitride crucible surface by heating Al chunks with 5 mol% of bismuth at 1273 K for 3 h under NH
3
gas flow. The fragments of the layer were characterized by X‐ray diffraction, scanning electron microscopy, and transmission electron microscopy. The platelet grains of AlN with a size of 0.1–1.0 μm and having preferred orientation of the
c
‐axis perpendicular to the layer were formed at the crucible side. Nanotubes 6–15 μm long and about 20–100 nm thick grew on the gas phase side of the layer. |
| Author | Ide, Tomoyuki Orikasa, Hironori Yamada, Takahiro Yamane, Hisanori Morito, Haruhiko Karahashi, Taiki |
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| Cites_doi | 10.1016/j.msea.2005.09.111 10.1016/j.jeurceramsoc.2003.12.028 10.1051/jp3:1993157 10.1016/0022-3697(73)90092-9 10.1016/S0022-0248(98)00819-7 10.1063/1.1482137 10.1016/S0955-2219(03)00014-1 10.1109/101.313460 10.1016/0955-2219(90)90050-P 10.1111/j.1151-2916.1993.tb06662.x 10.1016/0038-1098(77)90959-0 10.1016/j.jcrysgro.2005.02.040 10.1063/1.1663432 10.1111/j.1151-2916.1995.tb08357.x 10.1021/ie8011193 10.1002/9780470310496.ch50 10.1007/BF02868547 10.1107/S0365110X62002297 |
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| References_xml | – start-page: 8 volume-title: Smithells Metals Reference Book year: 1983 ident: e_1_2_5_23_2 contributor: fullname: James S. C. – ident: e_1_2_5_6_2 doi: 10.1016/j.msea.2005.09.111 – ident: e_1_2_5_16_2 doi: 10.1016/j.jeurceramsoc.2003.12.028 – ident: e_1_2_5_12_2 doi: 10.1051/jp3:1993157 – ident: e_1_2_5_2_2 doi: 10.1016/0022-3697(73)90092-9 – ident: e_1_2_5_19_2 doi: 10.1016/S0022-0248(98)00819-7 – ident: e_1_2_5_24_2 doi: 10.1063/1.1482137 – volume: 6 start-page: 1732 year: 1970 ident: e_1_2_5_17_2 article-title: Preparation of Gallium Nitride publication-title: Inorg. Mater. contributor: fullname: Pichugin I. G. – ident: e_1_2_5_15_2 doi: 10.1016/S0955-2219(03)00014-1 – volume: 28 start-page: 647 year: 1991 ident: e_1_2_5_11_2 article-title: Effect of LiF and BaF2 Addition on Synthesis of Fine AlN Powder publication-title: J. Kor. Ceram. Soc. contributor: fullname: Choi B. H. – volume: 125 start-page: 10176 year: 2003 ident: e_1_2_5_25_2 article-title: Synthesis and Characterization of Faceted Hexagonal Aluminum Nitride Nanotubes publication-title: J. Am. Ceram. Soc. contributor: fullname: Wu Q. – ident: e_1_2_5_3_2 doi: 10.1109/101.313460 – ident: e_1_2_5_10_2 doi: 10.1016/0955-2219(90)90050-P – ident: e_1_2_5_9_2 doi: 10.1111/j.1151-2916.1993.tb06662.x – ident: e_1_2_5_21_2 doi: 10.1016/0038-1098(77)90959-0 – volume: 9 start-page: 463 year: 1993 ident: e_1_2_5_5_2 article-title: Aluminium Nitride publication-title: Review of Synthesis Methods contributor: fullname: Selvaduray G. – ident: e_1_2_5_18_2 doi: 10.1016/j.jcrysgro.2005.02.040 – ident: e_1_2_5_4_2 doi: 10.1063/1.1663432 – ident: e_1_2_5_14_2 doi: 10.1111/j.1151-2916.1995.tb08357.x – volume: 72 start-page: 84 year: 1993 ident: e_1_2_5_13_2 article-title: A New Synthesis Process for AlN publication-title: Am. Ceram. Soc. Bull. contributor: fullname: Haussonne J. M. – ident: e_1_2_5_7_2 doi: 10.1021/ie8011193 – ident: e_1_2_5_8_2 doi: 10.1002/9780470310496.ch50 – ident: e_1_2_5_20_2 doi: 10.1007/BF02868547 – ident: e_1_2_5_22_2 doi: 10.1107/S0365110X62002297 |
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