Combustion Synthesis of ZrC-TiC Composite Nanoparticle by Self-Propagating High Temperature Synthesis (SHS) in ZrO2–TiO2–Mg/Al–C System
In this study, ZrC–TiC composite nanoparticle was synthesized by SHS method using oxide raw materials, carbon black, and Mg and Al reductants. For SHS processes, composite charge stoichiometriesStoichiometry were optimized for Mg usage, and the usage of Al and Mg was compared. The stoichiometriesSto...
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Published in | Advances in Powder and Ceramic Materials Science 2023 pp. 143 - 149 |
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Main Authors | , |
Format | Book Chapter |
Language | English |
Published |
Cham
Springer Nature Switzerland
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Series | The Minerals, Metals & Materials Series |
Subjects | |
Online Access | Get full text |
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Summary: | In this study, ZrC–TiC composite nanoparticle was synthesized by SHS method using oxide raw materials, carbon black, and Mg and Al reductants. For SHS processes, composite charge stoichiometriesStoichiometry were optimized for Mg usage, and the usage of Al and Mg was compared. The stoichiometriesStoichiometry of the chemicals used in the processes applied to remove undesired by-products and the most accurate process steps were determined for the purification of the SHS product. A novel route was established for purification of SHS product obtained by Al usage as reductant. Characterization was performed with XRD analysis. The results showed that commercial purity ZrC–TiC powder with high surface area could be synthesized by using both reductants. The results revealed that Mg is a better reductant, but Al with lower cost when compared to Mg is also a suitable reductant, although it increases the process steps. |
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ISBN: | 3031226216 9783031226212 |
ISSN: | 2367-1181 2367-1696 |
DOI: | 10.1007/978-3-031-22622-9_14 |