Influence of pH on the Formation of Sulfate and Hydroxyl Radicals in the UV/Peroxymonosulfate System
The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8–11, which could not be explained only by the generally accepted theory that SO4 •‑...
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| Published in | Environmental science & technology Vol. 45; no. 21; pp. 9308 - 9314 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Chemical Society
01.11.2011
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8–11, which could not be explained only by the generally accepted theory that SO4 •‑ was converted to HO• at higher pH. A hypothesis was proposed that the rate of PMS photolysis into HO• and SO4 •‑ increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (εPMS, 13.8–149.5 M–1·cm–1) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both HO• and SO4 •‑ at the pH range of 8–10. The formation of HO• and SO4 •‑ in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (SO5 •‑) and the conversion of SO4 •‑ to HO• by simulation and experimental results. Additionally, the apparent quantum yield for SO4 •‑ in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications. |
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| AbstractList | The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8-11, which could not be explained only by the generally accepted theory that ... was converted to ... at higher pH. A hypothesis was proposed that the rate of PMS photolysis into ... and ... increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (..., 13.8-149.5 ...) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both ... and ... at the pH range of 8-10. The formation of ... and ... in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (...) and the conversion of ... to ... by simulation and experimental results. Additionally, the apparent quantum yield for ... in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications. (ProQuest: ... denotes formulae/symbols omitted.) The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8–11, which could not be explained only by the generally accepted theory that SO4 •‑ was converted to HO• at higher pH. A hypothesis was proposed that the rate of PMS photolysis into HO• and SO4 •‑ increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (εPMS, 13.8–149.5 M–1·cm–1) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both HO• and SO4 •‑ at the pH range of 8–10. The formation of HO• and SO4 •‑ in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (SO5 •‑) and the conversion of SO4 •‑ to HO• by simulation and experimental results. Additionally, the apparent quantum yield for SO4 •‑ in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications. The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8-11, which could not be explained only by the generally accepted theory that SO(4)(•-) was converted to HO(•) at higher pH. A hypothesis was proposed that the rate of PMS photolysis into HO(•) and SO(4)(•-) increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (ε(PMS), 13.8-149.5 M(-1)·cm(-1)) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both HO(•) and SO(4)(•-) at the pH range of 8-10. The formation of HO(•) and SO(4)(•-) in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (SO(5)(•-)) and the conversion of SO(4)(•-) to HO(•) by simulation and experimental results. Additionally, the apparent quantum yield for SO(4)(•-) in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications. The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8-11, which could not be explained only by the generally accepted theory that SO(4)(•-) was converted to HO(•) at higher pH. A hypothesis was proposed that the rate of PMS photolysis into HO(•) and SO(4)(•-) increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (ε(PMS), 13.8-149.5 M(-1)·cm(-1)) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both HO(•) and SO(4)(•-) at the pH range of 8-10. The formation of HO(•) and SO(4)(•-) in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (SO(5)(•-)) and the conversion of SO(4)(•-) to HO(•) by simulation and experimental results. Additionally, the apparent quantum yield for SO(4)(•-) in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications.The influence of pH on the degradation of refractory organics (benzoic acid, BA) in UV(254 nm)/Peroxymonosulfate (UV/PMS) system was investigated. The degradation of BA was significantly enhanced at the pH range of 8-11, which could not be explained only by the generally accepted theory that SO(4)(•-) was converted to HO(•) at higher pH. A hypothesis was proposed that the rate of PMS photolysis into HO(•) and SO(4)(•-) increased with pH. The hypothesis was evidenced by the measured increase of apparent-molar absorption coefficient of PMS (ε(PMS), 13.8-149.5 M(-1)·cm(-1)) and photolysis rate of PMS with pH, and further proved by the increased quasi-stationary concentrations of both HO(•) and SO(4)(•-) at the pH range of 8-10. The formation of HO(•) and SO(4)(•-) in the UV/PMS system was confirmed mainly from the cooperation of the photolysis of PMS, the decay of peroxomonosulfate radical (SO(5)(•-)) and the conversion of SO(4)(•-) to HO(•) by simulation and experimental results. Additionally, the apparent quantum yield for SO(4)(•-) in the UV/PMS system was calculated as 0.52 ± 0.01 at pH 7. The conclusions above as well as the general kinetic expressions given might provide some references for the UV/PMS applications. |
| Author | Fang, Jing-Yun Ma, Jun Chen, Li-Wei Guan, Ying-Hong Li, Xu-Chun |
| AuthorAffiliation | Harbin Institute of Technology National Engineering Research Center of Urban Water Resources State Key Laboratory of Urban Water Resource and Environment |
| AuthorAffiliation_xml | – name: Harbin Institute of Technology – name: State Key Laboratory of Urban Water Resource and Environment – name: National Engineering Research Center of Urban Water Resources |
| Author_xml | – sequence: 1 givenname: Ying-Hong surname: Guan fullname: Guan, Ying-Hong – sequence: 2 givenname: Jun surname: Ma fullname: Ma, Jun email: majun@hit.edu.cn – sequence: 3 givenname: Xu-Chun surname: Li fullname: Li, Xu-Chun – sequence: 4 givenname: Jing-Yun surname: Fang fullname: Fang, Jing-Yun – sequence: 5 givenname: Li-Wei surname: Chen fullname: Chen, Li-Wei |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24712146$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/21999357$$D View this record in MEDLINE/PubMed |
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| Keywords | Benzoic acid Pollutant behavior Sulfates Pollution Ultraviolet radiation Carboxylic acid Hydroxyl radicals pH Environment Aromatic compound Organic compounds Photochemical degradation Inorganic radical anion |
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| Title | Influence of pH on the Formation of Sulfate and Hydroxyl Radicals in the UV/Peroxymonosulfate System |
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