Lanthanide–Organic Coordination Frameworks Showing New 5‑Connected Network Topology and 3D Ordered Array of Single-Molecular Magnet Behavior in the Dy Case
Five isostructural lanthanide–organic coordination frameworks with a unique 3-D 5-connected (47.63)(43.65.82) network, namely, [Ln(phen)(L)] n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3 L) and chelating 1,10-phen...
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| Published in | Inorganic chemistry Vol. 53; no. 13; pp. 6708 - 6714 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
07.07.2014
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| Online Access | Get full text |
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| Abstract | Five isostructural lanthanide–organic coordination frameworks with a unique 3-D 5-connected (47.63)(43.65.82) network, namely, [Ln(phen)(L)] n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3 L) and chelating 1,10-phenanthroline (phen) coligand. Significantly, the Dy(III) complex 1 is an organized array of single-molecular magnets (SMMs), with frequency-dependent out-of-phase ac susceptibility signals and magnetization hysteresis at 4 K. Further analysis of the magnetic results can reveal that the SMM behavior of 1 should arise from the smaller ferromagnetic interaction between the Dy(III) ions. Complex 1 was also characterized by X-ray absorption spectra, which give the clear X-ray magnetic circular dichroism signal. |
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| AbstractList | Five isostructural lanthanide-organic coordination frameworks with a unique 3-D 5-connected (4(7).6(3))(4(3).6(5).8(2)) network, namely, [Ln(phen)(L)]n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3L) and chelating 1,10-phenanthroline (phen) coligand. Significantly, the Dy(III) complex 1 is an organized array of single-molecular magnets (SMMs), with frequency-dependent out-of-phase ac susceptibility signals and magnetization hysteresis at 4 K. Further analysis of the magnetic results can reveal that the SMM behavior of 1 should arise from the smaller ferromagnetic interaction between the Dy(III) ions. Complex 1 was also characterized by X-ray absorption spectra, which give the clear X-ray magnetic circular dichroism signal.Five isostructural lanthanide-organic coordination frameworks with a unique 3-D 5-connected (4(7).6(3))(4(3).6(5).8(2)) network, namely, [Ln(phen)(L)]n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3L) and chelating 1,10-phenanthroline (phen) coligand. Significantly, the Dy(III) complex 1 is an organized array of single-molecular magnets (SMMs), with frequency-dependent out-of-phase ac susceptibility signals and magnetization hysteresis at 4 K. Further analysis of the magnetic results can reveal that the SMM behavior of 1 should arise from the smaller ferromagnetic interaction between the Dy(III) ions. Complex 1 was also characterized by X-ray absorption spectra, which give the clear X-ray magnetic circular dichroism signal. Five isostructural lanthanide-organic coordination frameworks with a unique 3-D 5-connected (4(7).6(3))(4(3).6(5).8(2)) network, namely, [Ln(phen)(L)]n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3L) and chelating 1,10-phenanthroline (phen) coligand. Significantly, the Dy(III) complex 1 is an organized array of single-molecular magnets (SMMs), with frequency-dependent out-of-phase ac susceptibility signals and magnetization hysteresis at 4 K. Further analysis of the magnetic results can reveal that the SMM behavior of 1 should arise from the smaller ferromagnetic interaction between the Dy(III) ions. Complex 1 was also characterized by X-ray absorption spectra, which give the clear X-ray magnetic circular dichroism signal. Five isostructural lanthanide–organic coordination frameworks with a unique 3-D 5-connected (47.63)(43.65.82) network, namely, [Ln(phen)(L)] n (Ln = Dy for 1, Gd for 2, Ho for 3, Er for 4, and Tb for 5), have been prepared based on bridging 5-hydroxyisophthalic acid (H3 L) and chelating 1,10-phenanthroline (phen) coligand. Significantly, the Dy(III) complex 1 is an organized array of single-molecular magnets (SMMs), with frequency-dependent out-of-phase ac susceptibility signals and magnetization hysteresis at 4 K. Further analysis of the magnetic results can reveal that the SMM behavior of 1 should arise from the smaller ferromagnetic interaction between the Dy(III) ions. Complex 1 was also characterized by X-ray absorption spectra, which give the clear X-ray magnetic circular dichroism signal. |
| Author | Sañudo, E. Carolina Chen, Min Du, Miao Jiménez, Erika Fang, Shao-Ming Liu, Chun-Sen |
| AuthorAffiliation | Tianjin Normal University College of Chemistry, Tianjin Key Laboratory of Structure and Performance for Functional Molecules, MOE Key Laboratory of Inorganic−Organic Hybrid Functional Material Chemistry European Synchrotron Radiation Facility Zhengzhou University of Light Industry Universitat de Barcelona Institut de Nanociència i Nanotecnologia i Departament de Química Inorgànica Henan Provincial Key Lab of Surface & Interface Science |
| AuthorAffiliation_xml | – name: College of Chemistry, Tianjin Key Laboratory of Structure and Performance for Functional Molecules, MOE Key Laboratory of Inorganic−Organic Hybrid Functional Material Chemistry – name: Universitat de Barcelona – name: Zhengzhou University of Light Industry – name: Henan Provincial Key Lab of Surface & Interface Science – name: Institut de Nanociència i Nanotecnologia i Departament de Química Inorgànica – name: European Synchrotron Radiation Facility – name: Tianjin Normal University |
| Author_xml | – sequence: 1 givenname: Min surname: Chen fullname: Chen, Min – sequence: 2 givenname: E. Carolina surname: Sañudo fullname: Sañudo, E. Carolina – sequence: 3 givenname: Erika surname: Jiménez fullname: Jiménez, Erika – sequence: 4 givenname: Shao-Ming surname: Fang fullname: Fang, Shao-Ming – sequence: 5 givenname: Chun-Sen surname: Liu fullname: Liu, Chun-Sen email: chunsenliu@zzuli.edu.cn – sequence: 6 givenname: Miao surname: Du fullname: Du, Miao email: dumiao@public.tpt.tj.cn |
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| Snippet | Five isostructural lanthanide–organic coordination frameworks with a unique 3-D 5-connected (47.63)(43.65.82) network, namely, [Ln(phen)(L)] n (Ln = Dy for... Five isostructural lanthanide-organic coordination frameworks with a unique 3-D 5-connected (4(7).6(3))(4(3).6(5).8(2)) network, namely, [Ln(phen)(L)]n (Ln =... |
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| Title | Lanthanide–Organic Coordination Frameworks Showing New 5‑Connected Network Topology and 3D Ordered Array of Single-Molecular Magnet Behavior in the Dy Case |
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