Copper-Catalyzed C(sp2)–S Coupling Reactions for the Synthesis of Aryl Dithiocarbamates with Thiuram Disulfide Reagents

An efficient protocol for the copper-catalyzed preparation of aryl dithiocarbamates from aryl iodides and inexpensive, environmentally benign tetraalkylthiuram disulfides was developed. The features of mild reaction conditions, high yields, and broad substrate scope render this new approach syntheti...

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Bibliographic Details
Published inOrganic letters Vol. 19; no. 21; pp. 5916 - 5919
Main Authors Dong, Zhi-Bing, Liu, Xing, Bolm, Carsten
Format Journal Article
LanguageEnglish
Published WASHINGTON American Chemical Society 03.11.2017
Amer Chemical Soc
Subjects
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
ISOTHIOCYANATES
EFFICIENT SYNTHESIS
CHEMISTRY
DERIVATIVES
ONE-POT
ANTIFUNGAL ACTIVITY
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Summary:An efficient protocol for the copper-catalyzed preparation of aryl dithiocarbamates from aryl iodides and inexpensive, environmentally benign tetraalkylthiuram disulfides was developed. The features of mild reaction conditions, high yields, and broad substrate scope render this new approach synthetically attractive for the preparation of potentially biologically active compounds.
Bibliography:ObjectType-Article-1
SourceType-Scholarly Journals-1
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ISSN:1523-7060
1523-7052
DOI:10.1021/acs.orglett.7b02911