A Versatile Preparative Route to 5-Substituted-1,10-Phenanthroline Ligands via 1,10-Phenanthroline 5,6-Epoxide
The reactive ligand 1,10-phenanthroline-5,6-epoxide is a versatile starting material for the preparation of a variety of 5-substituted-1, 10-phenanthroline ligands by reaction with oxygen-, carbon-, or nitrogen-based nucleophiles. All of the new ligands readily form complexes with the fac-Re-1(CO)(3...
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| Published in | Inorganic chemistry Vol. 34; no. 25; pp. 6235 - 6236 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
WASHINGTON
American Chemical Society
01.12.1995
Amer Chemical Soc |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The reactive ligand 1,10-phenanthroline-5,6-epoxide is a versatile starting material for the preparation of a variety of 5-substituted-1, 10-phenanthroline ligands by reaction with oxygen-, carbon-, or nitrogen-based nucleophiles. All of the new ligands readily form complexes with the fac-Re-1(CO)(3)Cl fragment. Of particular interest are the syntheses of the amino and aminocrown derivatives of Re-1 which can function as cation sensors by perturbation of molecular luminescence. An interesting example involving Pb2+ is presented. |
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| AbstractList | The reactive ligand 1,10-phenanthroline-5,6-epoxide is a versatile starting material for the preparation of a variety of 5-substituted-1, 10-phenanthroline ligands by reaction with oxygen-, carbon-, or nitrogen-based nucleophiles. All of the new ligands readily form complexes with the fac-Re-1(CO)(3)Cl fragment. Of particular interest are the syntheses of the amino and aminocrown derivatives of Re-1 which can function as cation sensors by perturbation of molecular luminescence. An interesting example involving Pb2+ is presented. |
| Author | Shen, Yibing Sullivan, B. Patrick |
| Author_xml | – sequence: 1 givenname: Yibing surname: Shen fullname: Shen, Yibing – sequence: 2 givenname: B. Patrick surname: Sullivan fullname: Sullivan, B. Patrick |
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| Snippet | The reactive ligand 1,10-phenanthroline-5,6-epoxide is a versatile starting material for the preparation of a variety of 5-substituted-1, 10-phenanthroline... |
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| SubjectTerms | Chemistry Chemistry, Inorganic & Nuclear Physical Sciences Science & Technology |
| Title | A Versatile Preparative Route to 5-Substituted-1,10-Phenanthroline Ligands via 1,10-Phenanthroline 5,6-Epoxide |
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