超高效液相色谱-串联质谱法测定牛奶中4种 β-内酰胺类抗生素及其主要代谢产物
目的 建立超高效液相色谱-串联质谱法检测牛奶中青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸含量的分析方法.方法 样品经0.2%氨水乙腈溶液超声离心提取,通过Oasis PRiME HLB固相萃取柱进行净化,采用超高效液相色谱-串联质谱法进行测定.结果 青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸在所考察的线性范围内线性良好,相关系数不低于0.999;方法 回收率为70.9%~101.6%,相对标准偏差(relative standard deviation,RSD)为4.0%~7.5%.市售的35份样品中,均未检出青霉素G、青霉素V、阿莫西林、氨苄西林及其代谢产...
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Published in | 食品安全质量检测学报 Vol. 12; no. 5; pp. 1662 - 1668 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | Chinese |
Published |
河北省疾病预防控制中心, 石家庄 050021
2021
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Subjects | |
Online Access | Get full text |
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Abstract | 目的 建立超高效液相色谱-串联质谱法检测牛奶中青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸含量的分析方法.方法 样品经0.2%氨水乙腈溶液超声离心提取,通过Oasis PRiME HLB固相萃取柱进行净化,采用超高效液相色谱-串联质谱法进行测定.结果 青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸在所考察的线性范围内线性良好,相关系数不低于0.999;方法 回收率为70.9%~101.6%,相对标准偏差(relative standard deviation,RSD)为4.0%~7.5%.市售的35份样品中,均未检出青霉素G、青霉素V、阿莫西林、氨苄西林及其代谢产物.结论 该方法操作简单、重现性好,可用于牛奶中青霉素G、青霉素V、阿莫西林、氨苄西林及其代谢产物脱羧噻唑酸的检测. |
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AbstractList | 目的 建立超高效液相色谱-串联质谱法检测牛奶中青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸含量的分析方法.方法 样品经0.2%氨水乙腈溶液超声离心提取,通过Oasis PRiME HLB固相萃取柱进行净化,采用超高效液相色谱-串联质谱法进行测定.结果 青霉素G、青霉素V、氨苄西林、阿莫西林及其代谢产物脱羧噻唑酸在所考察的线性范围内线性良好,相关系数不低于0.999;方法 回收率为70.9%~101.6%,相对标准偏差(relative standard deviation,RSD)为4.0%~7.5%.市售的35份样品中,均未检出青霉素G、青霉素V、阿莫西林、氨苄西林及其代谢产物.结论 该方法操作简单、重现性好,可用于牛奶中青霉素G、青霉素V、阿莫西林、氨苄西林及其代谢产物脱羧噻唑酸的检测. |
Author | 任贝贝 王丽英 秦振顺 路杨 常凤启 刘梦颖 |
AuthorAffiliation | 河北省疾病预防控制中心, 石家庄 050021 |
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Author_FL | WANG Li-Ying LIU Meng-Ying QIN Zhen-Shun REN Bei-Bei LU Yang CHANG Feng-Qi |
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DocumentTitle_FL | Determination of 4 kinds of β-lactam antibiotics and their main metabolites in milk by ultra performance liquid chromatography tandem mass spectrometry |
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Keywords | 超高效液相色谱-串联质谱法 牛奶 β-内酰胺类抗生素 |
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