Bicontinuous microemulsions for high yield, wet synthesis of ultrafine nanoparticles: a general approachElectronic supplementary information (ESI) available. See DOI: 10.1039/c5fd00004a

The design of a synthesis strategy for metal nanoparticles by templating dense microemulsions is proposed. Particle size is controlled by surfactant size rather than by microemulsion composition. The strategy was demonstrated with various systems with different surfactant: cationic, anionic and non-...

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Main Authors Latsuzbaia, Roman, Negro, Emanuela, Koper, Ger
Format Journal Article
LanguageEnglish
Published 16.07.2015
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Abstract The design of a synthesis strategy for metal nanoparticles by templating dense microemulsions is proposed. Particle size is controlled by surfactant size rather than by microemulsion composition. The strategy was demonstrated with various systems with different surfactant: cationic, anionic and non-ionic and of different sizes. Formulations were determined using the microemulsion phase diagrams. Synthesis was demonstrated for platinum nanoparticles with some examples for gold. The nanoparticles were subsequently extracted from the microemulsion by absorption onto a carbon support, after which the surfactant was recycled.
AbstractList The design of a synthesis strategy for metal nanoparticles by templating dense microemulsions is proposed. Particle size is controlled by surfactant size rather than by microemulsion composition. The strategy was demonstrated with various systems with different surfactant: cationic, anionic and non-ionic and of different sizes. Formulations were determined using the microemulsion phase diagrams. Synthesis was demonstrated for platinum nanoparticles with some examples for gold. The nanoparticles were subsequently extracted from the microemulsion by absorption onto a carbon support, after which the surfactant was recycled.
Author Negro, Emanuela
Koper, Ger
Latsuzbaia, Roman
AuthorAffiliation Delft University of Technology
Department of Chemical Engineering
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  givenname: Ger
  surname: Koper
  fullname: Koper, Ger
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Electronic supplementary information (ESI) available. See DOI
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  end-page: p 535-576
  publication-title: Intermolecular and Surface Forces
  doi: Israelachvili
– issn: 2005
  end-page: p 1-3
  publication-title: Nanoparticles
  doi: Schmid
– issn: 2012
  publication-title: Surfactants and Interfacial Phenomena: Fourth Edition
  doi: Rosen Kunjappu
– issn: 2004
  publication-title: Mesophases, Polymers, and Particles
  doi: Lagaly Richtering Hauptversammlung
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Title Bicontinuous microemulsions for high yield, wet synthesis of ultrafine nanoparticles: a general approachElectronic supplementary information (ESI) available. See DOI: 10.1039/c5fd00004a
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